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029 <br />Work Order: 09-8452 <br />Client Project ID: <br />ANALYTICAL QC SUMMARY REPORT <br />BatchlD: 21283 <br />Sample ID: LCS-21283 SampType: LCS TestCode: 200.7_D Run ID: ICP-0PTIMA 6300 DV 091024A Prep Date: 10/23/2009 Units: mg/L <br />Batch ID: 21283 TestNo: E200.7, Rev. FileID: 102409AM Analysis Date: 10/25/2009 SegNo: 928667 <br />knalyte Result . LQL SPK value SPK Ref Val %REC Lowl-imit Hlghl-imit RPD Ref Val %RPD RPDLimit Qual <br />Cobalt 1,994 0.00500 2 0 99.7 85 115 0 0 <br />Iron 5.746 0.0700 5 0 115 85 115 0 0 <br />Lithium 1.908 0.00200 2 0 95.4• 85 115 0 0 <br />Magnesium 10.04 0.150 10 0 100 85 115 0 0 <br />Manganese 2.027 0.00500 2 0 101 85 115 0 0 <br />Nickel 2.043 0.0300 2 0 102 85 115 0 0 <br />Potassium 9.526 0.340 10 0 95.3 85 115 0 0 <br />Silver 0.1922 0.0300 0.2 0.00403 96.1 80 115 0 0 <br />Sodium 9.679 0.400 10 0 96.8 85 115 0 0 <br />Vanadium 2.144 0.0100 2 0 107 85 115 0 0 <br />Zinc 2.014 0,0300 2 0 101 85 115 0 0 <br />Silicon as Si02(SIIIca) 10.82 0.107 10.65 0.04418 102 77.3 115 0 0 <br />Sample ID: 09-8452-01AMS SampType: MS TestCode: 200.70 Run ID: ICP-OPTIMA 6300 DV 091024A Prep Date: 10/23/2009 Units: mg/L <br />client ID: MW-002 Batch ID: 21283 TestNo; E200.7, Rev. FileID: 102409AM Analysis Date: 10/26/2009 SegNo: 928669 <br />knalyte Result LQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Aluminum 2.701 0.125 <br />Barium 5.611 0.00250 <br />Beryllium 0.06708 0.000563 <br />Boron 3,089 0.0250 <br />Calcium 275.6 0.484 <br />Chromium 2.506 0.0125 <br />Cobalt 2.438 0.00625 <br />Iron 6.744 0.0875 <br />Lithium 2.613 0.00250 <br />Magnesium 93.27 0.188 <br />Manganese 3.261 0.00625 <br />Nickel 2.53 0.0375 <br />Potassium 19.24 0.425 <br />Silver 0.2679 0.0375 <br />Qualifiers: U - Not detected at or above the Reporting Limit <br /> J - Analyte detected below quantitation limits <br /> S - Spike Recovery outside acceptance limits <br /> E - Extrapolated value, value exceeds calibrat ion range. <br />2.5 0.04374 108 75 <br />6.25 0.05122 89 75 <br />0.0625 0.006357 97.2 75 <br />2.5 0.1518 118 75 <br />12.5 253.5 177 75 <br />2.5 0 100 75 <br />2.5 0 97.5 75 <br />6.25 0.04117 108 75 <br />2.5 0,09731. 101 75 <br />12.5 78.88 115 75 <br />2.5 0.7967 98.6 75 <br />2.5 0 101 75 <br />12.5 6.883 98.9 75 <br />0.25 0 107 75 <br />R - RPD outside acceptance limits <br />B - Analyte detected in the associated Method Blank <br />H - Prep or analytical holding time exceeded <br />X - See case narrative <br />125 0 0 <br />125 0 0 <br />125 0 0 <br />125 0 0 <br />125 0 0 <br />125 0 0 <br />125 0 0 <br />125 0 0 <br />125 0 0 <br />125 0 0 <br />125 0 0 <br />125 0 0 <br />125 0 0 <br />125 0 0 <br />S <br />