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028 <br />Evergreen Analytical, Inc. <br />Work Order: 09-8452 <br />Client Project ID: <br />Date: 02-Nov-09 <br />ANALYTICAL QC SUMMARY REPORT <br />BatchID: 21283 <br />Sample ID: MB-21283 SampType: MBLK TestCode: 200.7_D Run ID: ICP-OPTIMA 5300 OV_091024A Prep Date: 10/23/2009 Units: mg/L <br />Batch ID: 21283 TestNo: E200.7, Rev. FileID: 102409AM Analysis Date: 10125/2009 SegNo: 928664 <br />Analyte Result LQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />AI..... i....? <br /> V UAVU <br />Barium U 0.00200 <br />Beryllium U 0.000450 <br />Boron U 0.0200 <br />Calcium U 0.387 <br />Chromium U 0.0100 <br />Cobalt U 0.00500 <br />Iron U 0.0700 <br />Lithium U 0.00200 <br />Magnesium U 0.150 <br />Manganese U 0.00500 <br />Nickel U 0.0300 <br />Potassium U 0.340 <br />Silver U 0.0300 <br />Sodium U 0.400 <br />Vanadium U 0.0100 <br />Zinc U 0.0300 <br />Silicon as Si02(Silica) U 0.107 <br />Sample ID: LCS-21283 SampType: LCS TestCode: 200.7D Run ID: ICP-OPTIMA 5300 DV 091024A Prep Date: 10/23/2009 Units: mg/L <br />Batch ID: 21283 TestNo: E200.7, Rev. FileID: 102409AM Analysis Date: 10125/2009 SegNo: 928667 <br />Analyte Result LQL SPK value SPK Ref Val %REC Lowl-imit Hight-imit RPD Ref Val %RPD RPDLimit Qual <br />w-1-11i i.tstso u,tuu <br />Barium 4.852 0.00200 <br />Beryllium 0.053 0.000450 <br />Boron . 2.163 0.0200 <br />Calcium 10.24 0.387 <br />Chromium 2.05 0.0100 <br />Qualifiers: U - Not detected at or above the Reporting Limit <br /> J - Analyte detected below quantitation limits <br /> S - Spike Recovery outside acceptance limits <br /> E - Extrapolated value, value exceeds calibration range. <br />2 0 99.4 85 115 <br />5 0 97 85 115 <br />0.05 0 106 85 115 <br />2 0 108 85 115 <br />10 0 102 85 115 <br />2 0 103 85 115 <br />R - RPD outside acceptance limits <br />B - Analyte detected in the associated Method Blank <br />H - Prep or analytical holding time exceeded <br />X - See case narrative <br />0 0 <br />0 0 <br />0 0 <br />0 0 <br />0 0 <br />0 0