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030 <br />Work Order: 09-8452 <br />Client Project ID: <br />ANALYTICAL QC SUMMARY REPORT <br />BatchID: 21283 <br />Sample ID: 09-8452-01AMS SampType: MS TestCode: 200.7_D Run ID: ICP-OPTIMA 5300 DV 091024A Prep Date: 10/23/2009 Units: mg/L <br />Client ID: MW-002 Batch ID: 21283 TestNo: E200.7, Rev. FileID: 102409AM Analysis Date: 10/2612009 SegNo: 928669 <br />Analyte Result LQL SPK value SPK Ref Val %REC Lowlimit Hig hLimft RPD Ref Val %RPD RPDLimit Qual <br />Sodium 194.4 0.500 12.5 189.8 37.1 75 125 0 0 S <br />Vanadium 2.712 0.0125 2.5 0 108 75 125 0 0 <br />Zinc 2.363 0.0375 2.5 0 94.5 75 125 0 0 <br />Silicon as Si02(Silica) 33.36 0.134 13.38 18.24 113 75 125 0 0 <br />Sample ID: 09-8462-01AMSD SampType: MSD TestCode: 200.7_D Run ID: ICP-OPTIMA 5300 DV 091024A Prep Date: 10/23/2009 Units: mg/L <br />Client ID: MW-002 Batch ID: 21283 TestNo: E200.7, Rev. FileID: 10240DAM Analysis Date: 10/26/2009 SegNo: 928670 <br />Analyte Result LQL SPK value SPK Ref Val %REC Lowlimit Hig hLimit RPD Ref Val %RPD RPDLimit Qual <br />Aluminum 2.704 0.125 2.5 0.04374 108 75 125 2.805 3 <br />65 20 <br />Barium 5,549 0.00250 6.25 0:05122 88 75 125 6.32 . <br />13 <br />0 20 <br />Beryllium 0.06692 0.000563 0.0625 0.006357 96.9 75 125 0.07681 . <br />13.8 20 <br />Boron 3.034 0.0250 2.5 0.1518 115 75 125 3 1 <br />10 20 <br />Calcium 271.7 0.484 12.5 253.5 146 75 125 267.3 . <br />61 <br />1 20 S <br />Chromium 2.461 0.0125 2.5 0 98.4 75 125 2.358 . <br />4 <br />26 20 <br />Cobalt 2.399 0.00625 2.5 0 96 75 125 2.349 . <br />11 <br />2 20 <br />Iron 6.822 0.0875 6.25 0.04117 109 75 125 6.672 . <br />2 <br />23 20 <br />Lithium 2.586 0.00250 2.5 0.09731 99.6 75 125 2.974 . <br />14 <br />0 20 <br />Magnesium 92.94 0.188 12.5 78.88 113 75 125 96.31 . <br />3 <br />56 20 <br />Manganese 3.203 0.00625 2.5 0.7967 96.3 75 125 3.155 . <br />1 <br />51 20 <br />Nickel 2.488 0.0375 2.5 0 99.5 75 125 2.425 . <br />2.60 20 <br />Potassium 19.07 0.425 12.5 6.883 97.5 75 125 21.73 13 <br />0 20 <br />Silver 0.263 0.0375 C.25 0 105 75 125 0.2598 . <br />1.21 20 <br />Sodium 189.4 0.500 12.5 189.8 -3.1 75 125 212.8 11.7 20 S <br />Vanadium 2.67 0.0125 2,5 0 107 75 125 2.575 3.64 20 <br />Zinc 2.313 0,0375 2.5 0 92.5 75 125 2.255 2 <br />53 20 <br />Silicon as Si02(Silica) 33.33 0.134 13.38 18.24 113 75 125 0 . <br />0 <br /> 20 <br />ualitiers: U - Not detected at or above the Reporting Limit R - RPD outside acceptance limits <br /> J - Analyte detected below quantitation limits B - Analyte detected in the associated Method Blank <br /> S - Spike Recovery outside acceptance limits H - Prep or analytical holding time exceeded <br /> E - Extrapolated value, value exceeds calibration range. X - See case narrative <br />