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Key Laboratories, Inc. <br />Client: Walsh Environmental 2479A Riverside Parkway <br />Client Project Name : New Horizon Mine Grand Junction, Colorado 81505-1319 <br />Client Project Number: 900882.0001.010 Phone (970) 243-5311 Fax (970) 243-6010 <br />Client Sample Number: NHSS-239A <br />Client Sample Location: New Horizon Mine. 0-24 Key Lab a: t0-1024 <br />Sampling Date : 7/15/2010 Work Order k : 0716101002 <br />Sampling Time: <br />Sample Matrix . Soil Date Received: <br />Analyst: 07116/10 r•v/??) r <br />JI'Ll L <br />Sampler: Edward Sample Prep: Total, Open Vessel <br />Analysis Method : •ICP-MS, EPA Methods 60201200rbp Method: EPA Method 200.8 Open Vessel Microwave Digestion <br />Wednesday, Wednesday, <br />Date Analyzed: July 21, 2010 July 21, 2010 <br />23:53:03 20:14:39 <br />Key Lab Prep Batch Sample IDH Wi•07208.10- Wi-0720B-10- <br />1024-141X10% 0000-01 LMB <br />Sample Comments: LMB <br />Sample Aliquot jmg]: 1071,1 1000 <br />Prep Au Spike Recovery: 1,001 0.983 <br />Prep/Digestion DN-» 46.68 50 <br />Page A of ss» T-1 nv-" Af:e ei <br /> Arn*sls ton Tim, svalew RcRa Audit Anal a Reported Value Units Method Blank Blank DF MDL <br />Method Mass umir• ppm PQL ppm Max OL ppm <br /> I <cea p Analytes Reported <br />ecXMS• 7 100 Le Lithium mVKg 500.00 0.25 1 500 <br />icP.MS• a ,o Be Beryllium mgn(g < < < <br />icr'MS' 1t tco B 11 Boron mg1Kg 500.00 0.6 2 500 <br />icP.us• 23 le Ng Sodium mg1Kg < < < <br />icP-MS• - Mg MA neslnm mg/Kg < c c <br />a-Mr a7 a AI Aluminum mg/Kg < < < <br />icP.w• zs w Si silicon mg/Kg < < < <br />rcw2s• 31 to p Phosphorus mg/Kg < < c <br />ICRMe• 39 1. K Potassium mg/Kg < < < <br />e,'Ma• r. 20 CA Calcium mg7Kg < < < <br />icrMS• ee 10 Ti Titanium mg1Kg < < c <br />?GP•Ma• 51 10 V Vanandium m91K9 <br />< <br />< <br />< <br />ieo-us• e2 1e Cr 100 Chromium mg1Kg e < < <br />KP•MS• 5s 10 Mn Manganese mg1Kg < c < <br />rcP.Ma• 5e 20 Fe Iron mg1Kg < c < <br />icP.MS• ss +o Co Cobalt mglKg c < < <br />1CPMa• W +o Ni Nickel mg1Kg < < < <br />mP.w- 0 1o Cu Copper mg/Kg < < < <br />lcp.s. ss m Zn Zinc mg1Kg < < < <br />1—— 75 +°o As 100 Arsenic mg/Kg 600.00 0.45 118 1000 <br />lcp?Mr a2 too Sc 20 x Selenium 0.2 J mg/Kg < 500.00 0.15 0.6 1000 <br />icpMS• ae ,ro Sr Strontium mg1Kg 500.00 0.025 0.1 1000 <br />op-"s' as o MO Molybdenum mg/Kg < < < <br />icPalr 107 1o Ag 100 Silver mglKg < c < <br />rcP-MS• /n +o Cd 20 Cadmium mg/Kg < < < <br />ICp'M6' 123 b Sb Antimony mg/Kg < < < <br />icP'Ms' 137 too Ba 2000 Barium mg/Kg 600.00 0,03 0.12 1000 <br />rc".- 2os 1s Hg 4 Mercur mg1K9 < < c <br />tal'us• am 1o T] Thalifum mg/Kg < c < <br />lc -Me• me o Pb 100 Lead mg/Kg < < < <br />icP.us• 232 1m Th Thorium mg/Kg 600.00 01005 0.02 600 <br />mP.Ms• na hod U Uranium moixg 600.00 O.ODb 0.02 500 <br /> <br />Notes: LMB= laboratory method blank, M and MD -sample matrix replicates <br />Notes: LCS =spiked laboratory method blank, MS and MSD - spiked sample matrix replicates <br />Notes: Au Is spiked as sample prep surrogate and to facilitate analysis of Mercury, DF - Dilution Factor, <br />Notes: MDL - Method Detection Limlk PQL= primaryQuantitation Limit, MCIL= Maximum Quantttatlon Limit, <br />Notes: <- less than MDL, J = Greater than MDL but less than PQL (4 x MDL), E -Estimated Value because It exceeds the MOL <br />Notes: n.a. - Not Applicable, Blank Space se Not Requested or Not Reported <br />Notes: RCRA TCLP Extract Limits: Ba =100 ppm; ICr, As,Ag,Pb] 1.5ppm; [Se, Cd] = 1 ppm; Hg • 0.2 ppm <br />Notes: "`(Total RCRA limits) are 20 times the TCLP extract limits because of TCLP sample size (100g) and extract volume (2000mL). <br />""EPA S W 646 Method 1311, Revision 0, July 1992, Section 1.2: "If a total lutalysis of the waste demonstrates that individual analytes sre, not present in the waste, <br />or that they are present but at such low conccntraliolre them the appropriate regulatory levels could not possibly be exceeded, the TCLP need not be run." <br />Analyst / Reviewer <br />