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Key Laboratories, Inc. <br />Client; Walsh Environmental 1-479A Riverside Parkway <br />Client Project Name: New Horizon Mine Grand Junclinn, Colorado 81505-1319 <br />Client Project Number: 900882,0001.010 Phone (970) 243-5311 Fax (970) 243-6010 <br />Client Sample Number: NHSS-239B <br />Client Sample Location: New Horizon Mine. 24-48 Key Lab e: 10-1025 <br />Sampling Date : 711512010 Wort: order :: 0716101002 <br />Sampling Time: Daze Received: 07116110 <br />6ampk Mavix ; Soil alalyst <br />Smnpler: Edward Sample Prep: Total, Open Vase) <br />Analysis Method : -ICP-MS, EPA Methods 6020 f 200kp Method: EPA Method 200.8 Open Vessel Microwave Digestion <br /> Wednesday, <br />Date Analyzed: July 21, 2010 <br />23:58:47 Wednesday, <br />July 21, 2010 <br />20:14:39 <br /> Key Lab Prep Batch Sample IDN W607208-10- <br />1026-15 IX10X <br />Sample Comments: <br />Sample Aliquot 1mg1: 1065.6 <br />Prep Au Spike Recovery: 1.016 <br />Prep/Digestion DFm» 46.92 <br />Pass Audit +=» x Total DF-->> 469.22 WI-0720B-10- <br />0000-01 LM8 <br />LMB <br />1000 <br />01983 <br />50 <br />500.00 <br /> °n?y'ta ton <br /> <br />Method Masa r'l- symlwl RCAA <br />.W- Audit Ana a <br />tIma• hd <br />Reported Value Units <br />Method Blank <br />Slank DF MDL <br />ppm PQL ppm Max QL ppm <br /> 1 <<=- If Analytes Reported <br /> as.MS• r IN Li Lithium mg/Kg 500.00 0.25 1 500 <br /> IcP-MS• a +o Be Beryllium mg/Kg c < c <br /> x:a.s• ,I +aa B Boron mgfKg 500.00 0.5 2 Soo <br /> Ice-MS• as w Na Sodium mgfKg < < e <br />10r+Ms• 2, to Mg Magnesium mgfKg e < < <br />IcP-us• v 1- Al Aluminum mgfKg c < c <br />Icr-us• 2. to Si Silicon mgfKg < c < <br />kRMS• 31 to p Phosphorus mglxg < < < <br />kP-.s• 2e +0 1C Potassium mglKg < < < <br />tcp-Ms• ,4 20 Ca Calcium mgfKg < < < <br />I—— ,a to Ti Titanium mgfKg < < < <br />tcP-Ma' s, Ia V Vanandium mg/Kg < c < <br />ICP-Ms' 52 to Cr 100 Chromium mgfKg < < e <br />ICP-MS• 65 to Mll Manganese mg/Kg < < < <br />s, 20 Pe Iron mgfKg < < < <br />IcPS• ss to Co Cobalt mgfKg < < < <br />kP-tur ce lo Ni Nickel mg/Kg < < < <br />IORMS• 63 to Cu Copper mgfKg < < < <br />IraMS• ss ro Zn ZinC mglKg < < < <br />w-m- rs IN As 100 Arsenic mgfKg 600.00 0.46 1.8 tooo <br />""s' 92 too Se 20 x Selenium < mgfKg < 600.00 0.15 0.8 1000 <br />1CP-Ma• ae I N Sr Strontium M&IRg 600,00 0.025 0,1 1000 <br />100..8' 1.m MO Molybdenum mg/Kg < < < <br />ICPMa' 107 fa A 100 Silver mgfKg < < < <br />ICP-M6• 111 10 Cd 20 Cadmium mgfKg < < < <br />1.11 • <br />I ll Antimony mgfKg < < < <br />'cP Me' % 2000 Barium m91Kg 500.00 0.03 0,12 1000 <br />1cP.MS• 4 Mercury mgfKg < < <br />1 oTl Thallium mg1Kg < < < <br />-ms- 2- to Pt, 100 Lead mgfKg c < < <br />10"..r 232 100 Th T horium mg/Kg 500.00 0.005 0.02 Soo <br />41.3• 238 IN U U ranium mgMg 600.00 0.005 0.02 500 <br />-Typically, all metals with - 901ms( Integt alion time can be reported. Available at customer's request. <br />Notes: LMB = laboratory method blank, M and MD - sample matrix replicates <br />Notes: LCS = spiked laboratory method blank, MS and MSD= spiked sample matrix replicates <br />Notes: All is spiked as sample prep surrogate and to facilitate analysis of Mercury, DF = Dilution Factor, <br />Notes: MDL - Method Detection Limit, PQL= Primary Quantitation Urnit, MQL - Maximum Quantitatlon Limit, <br />Notes: <- less than MDL, J or Greaterthan MOL but less than PQL (4 x MDL), E -Estimated Value because It exceeds the MQL <br />Notes: n.a. = Not Applicable, Blank Space = Not Requested or Not Reported <br />Notes: RCRA TCLP Extract Limits: Ba =100 ppm; [Cr, As,AlhPb[ - 5ppm; [Se, Cd) - 1 ppm; Hg - 0.2 ppm <br />Notes: ''(Total RCRA limits) are 20 times the TCLP extract limits because of TCLP sample size (100g) and extract volume (2000mL). <br />'-EPA S V/946 Method 1311, Revision 0. July 1992, Section 1.2! 'Ira teal analysis ofthe wash demonstrates that individual anatyta are not present in the waste, <br />or that they are present but at such low concentrations that the appropriate regulatory levels could not possibly be exceeded, the TCLP treed rat be run.' <br />Analyst/ Reviewer <br />