2010-08-18_ENFORCEMENT - C1981008

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Key Laboratories, Inc. Client: Walsh Environmental 2479A Riverside Parkway Client Project Name: New Horizon Mine Grand Junction, Colorado 81505-1319 Client Project Number: 900882.0001.010 Phone (970) 243-5311 Fax (970) 243-6010 Client Sample Number: NHSS-23811 Client Sample Location: New Horizon Nfine, 2448 Ivey Lab k: 10-1013 Sampling Dole: 7/1512010 Work Order 0716101002 Sampling Tama: Sample,Malrix: Soil Date Received: Analyst : 07116110 1 - \ t -71 J?j Z?l 1 Sampler: Edward Sample Prep: Y Total, Open Vessel Analysis Method : "ICP-MS, EPA Methods 6010 / 20Rthp Method: EPA Atethod 200. 8 Open Vessel Micleaove Digestion Date Analyzed; July 21, 2010 July 21, 2010 23:47:16 20:14:39 Key Lab Prep Batch Sample ID# WI.0720B-10- Wi•07206-10- 1023.131X10X 0000.01 LMB Sample Comments: LMB Sample Aliquot 1mgl: 1088.1 1000 Prep Au Spike Recovery; 0.991 0.983 Prep/Digestion DF=» 45.95 s0 Pass Audit==» x Total DF==>> 459.52 SDo.Oo analyals Ion nmv sml aeaa Audit AnalYte Reported Value Units Method Blank Blank OP MOL ppm PQL ppm Max QL ppm 1 c<==# Analytes Reported ICP-MS' 7 1W Li Lithium mgfKg 500.00 0.25 1 600 ICP-NS• 5 111 Be Beryllium mg/Kg < < C -W- 11 too B Boron mgJKg 5110.00 0.6 2 Soo ICP-Ms' 23 ut Na Sodium mg/Kg < < < IcP.us• 24 1. Mg Magnesium mgfKg < < < IcP-Ns• 2? to Al Aluminum mglK4 < < c ICPMS• 28 to Si Silicon mgJKg < < ICP#15' al 1p P Phosphorus mgfKg < < < lcP-MS• aP m g Potassium mgfKg < c < ILP-MS• 14 20 C}t Calcium mgAtg < < IcP-ms' 4e 10 Titanium mg1Kg < < < ICPMS• 51 10 V Vanandium mgfKg < < ICP-ms. 62 to Cr 100 Chromium mg1Kg < < < nF`_- 35 10 Mn Manganese mgJKg < < < .F`Ms• s, m Fe Iron mgfKg < < < Icwets• sa 10 Co Cobalt mgfKg < < < ICP•Ma• 9o to Ni Nickel mgfKg < < < icP.ua• w 111 Cu Co Cl' mgJKg < < ICPMS- m 111 Zit Zinc mgfKg < < < iGPMa• r5 loo As 100 Arsenic mg/Kg SOD,00 0.45 1.8 1000 ICPMS• e2 too Se 20 x Selenium 0.4 J mg/Kg < 500.00 0.15 0.6 1000 IcP-2.15• as loo Sr Strontium mgJK g sao.1111 0.025 0-1 1000 icP.M3• se Q MO Mol bdenum mgfKg < < ICPMS' lei to A 100 Silver mg/Kg < < < Ic0.M3• 111 10 Cd 20 Cadmium mg/Kg < < IC0.M5' 123 10 Sb Antimony mgfKg c < < 132 100 BI 2000 Barium mg/Kg 500.00 0.03 0.12 1000 iw-MS• 202 to FI 4 Mercury mgfKg < < < IcP-rns• ms 111 TI Thallium T:i mgJKg < < < ,cP.MS• zoo m Pb 100 Lead mglKg < < < ICPMs' 232 1W Th Thorium mg/Kg 500.00 0.005 0.02 Soo IcP-Ms. 23e too [J Uranium mgJKg 500.00 0.005 0.02 500 'Typically, ail metals wifb - 901rus] integration time can be reported Available at customer's rcoucst. Notes: LMB =laboratory method blank, M and MD =sample matrix replicates Notes: LCS = spiked laboratory method blank, MS and MSD - spiked sample matrix replicates Notes: Au Is spiked as sample prep surrogate and to facilitate analysis of Mercury, DF = Dilution Factor, Notes: MDL - Method Detection Limit, PQL a primary Quantitation Limit, MOL = Maximum Quantitation Limit, Notes: < = less than MDL, J - Greater then MDL but less than PQL (4 x MDL), E -Estimated Value because It exceeds the MQL Notes: n.a. = Not Applicable, Blank Space • Not Requested or Not Reported Notes: RCRA TCLP Extract Limits: Ba = 100 ppm; [Cr, As,A9,Pb] - 5ppm; [Se, Cd] = 1 ppm; Hg = 0.2 ppm Notes: "(Total RCRA limits) are 20 times the TCLP extract limits because of TCLP sample size (100g) and extract volume (20DOmL). "'EPA S W846 Method 1311, Revision O, July 1992, Section 1.2! "It. toted analysis of the waste demonstrates that individual analytes arc not present in the waste, or that they are present but at such low con eatradons that the appropriate regulatory levels could not possibly be exceeded, the TCLP need net be run." Analyst/ Reviewer