2010-08-18_ENFORCEMENT - C1981008

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Client : Walsh Environmental Client Project Name: New Horizon Mine Client Project Number: 900882.0001.010 Client Sample Number: NHSS-239A Client Sample Location: New Horizon Mine, 0-24 Sampling Date : 7/1512010 Sampling Time: Sample Matrix: Soil Sampler: Edward Analysis Method: 'ICP-MS, EPA Mclhods 6010 / 200rbp Method: Key Laboratories, Inc. 2479A Riverside Parkway Grand Junction, Colorado 81505-1319 Phone (970) 243-5311 Fax (970) 243-60 10 Frey Lab C: 10-1022 Work Order a: 0716101002 Date Received: 07116/10 ! f Z? i Analyst: -7 Sample Prep : Total, Open Vessel EPA Method 200.8 Open Vessel Microwave Digestion Wednesday, Date Analyzed: July 21, 2010 23:41:31 Wednesday, July 21, 2010 20:14:39 Key Lab Prep Batch Sample IDH WI.07208-10- 1022-121X10X Sample Comments: Sample Aliquot iengl: 1020,5 Prep An Spike Recovery: 1.021 Prep/Digestion DF^» 49.00 Pass Audlt==» x Total DF=>> 489.96 Wi-0 72 0 8-10- 0000.01_LMB LMB 1000 0.983 50 500.00 AnalyMS Method Ion Ttms RCRA Mass I. aymbpl l.lmtl„ Audit Analyte Reported Value Units Method Blank Blank DF MDL ppm PQL ppm Max QL ppm I <<== N Analytes Reported IcP-Ma• r loo Li Lithium mg1Kg 5D0.00 0.25 1 500 IMIns• 9 10 Be Beryllium mg/Kg < < < r,`Ms• 11 1co B Boron mg/Kg 500.00 0.6 2 600 -MS. 23 1. Na Sodium mg/Kg < < < Icp,As- 24 to Mg Magnesium mgfKg < < < 1Cr-Ma• n to Al Aluminum mgfKg < < < IC0.Ma• m 10 Si Silicon mglKg < < < ICP-Ms• 31 10 p Phosphorus mg1Kg < < < IOP-MS• ae 10 ]{ Potassium mgfKg < ICP-MS• 41 20 Ca Calcium mgfKg < icw-MS• 4e 10 Ti Titanium mgfKg < IewMS• m to V Vanandium mg/Kg < < < IV-MS• 52 to Cr 100 Chromium mg/Kg < < < tcp-MS• a5 10 Mn Manganese mglxg < < c IC0.MS' 54 m Fe Iron mg/Kg < c c ICP-Ms• so +o Co Cobalt mg/Kg < e e Ice-a1r m In Ni Nickel mg/Kg < < < Icp+w• at In Cu Copper mg/Kg c < c Ie0.M9' 66 10 Zn Zinc mg/Kg < < < taP-MS• ra 100 As 100 Arsenic mg1K9 500.00 0.45 1.8 1000 IcP-MS• 62 100 Se 20 x Selenium 0.27 .1 mgfKg < 600,00 0.15 0.6 1000 lCPM3• a5 100 Sr Strontium mgfKg 500.00 0.025 0,1 1000 ICP-Ma• 90 In Mo Molybdenum mgfKg < < < Icp.M3• ter 1. Ag 100 Silver mg/Kg < < ` IeP-14s. 111 10 Cd 20 Cadmium mg/Kg < < ` ICPMS• 123 In Sb Antimony mg/Kg < < < CP-Ma• ,37 Ba 2000 Barium mgfKg 600.00 0.03 0.12 1000 Icp-Ma• Hg 4 Mercury mg/Kg < < < IGPMS• 205 In TI Thallium mgfKg < < < ILP-MS• oat 1. Pb 100 Lead mg1K9 < < < x:p-ms• 211 100 Th Thorium mg/Kg 600.00 0.006 0.02 600 "P... 2 140 U Uranium mgrKg 500.00 0.005 0.02 500 . . aTypicnlly, xll metais wid. - 901nis) integration time can be reported. Available fit customer's request. Notes: LMB = laboratory method blank, M and MD - sample matrix replicates Notes: LCS = spiked laboratory method blank, MS and MSD= spiked sample matrix replicates Notes: Au Is spiked as sample prep surrogate and to faellNate analysis of Mercury, DF = Dilution Factor, Notes: MDL • Method Detection Limit, PQL - Primary Quantltation Llmtt, MOL= Maximum Quantitation Limit, Notes: <- less than MDL, J- Greater than MDL but less than PQL (4 x MDL), E -Estimated Value because It exceeds the MOIL Notes: n.a, = Not Applicable, Blank Space = Not Requested or Not Reported Notes: RCRA TCLP Extract Limits: Ba =100 ppm; lCr, As,Ag,Pb1= 6ppm; (Se, Cdl - 1 ppm; Hg v 0.2 ppm Notes: "(Total RCRA limits) are 20 times the TCLP extract limits because of TCLP sample size (1009) and extract volume (2000ml.), "EPA SW 846 Method 1311. Revision 0, July 1992, Section 11: "If a total analysis of the waste demonstrates diet individual analytes are not present in the waste, or that they ere present but at such low concentrations that the appropriate regulatory levels could not possibly be exceeded, the TCLP need not be run." Analyst/ Reviewer