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Key Laboratories, Inc. <br />Client: Walsh Environmental 2479A Riverside Parkway <br />Client Project Name : New Horizon Aline Grand Junction, Colorado 61505-1319 <br />Client Project Number : 900882.0001.010 Phone (970) 243-5311 Fax (970) 243-6010 <br />Client Sample Number: NHSS-2378 <br />Client Sample Location : New Horizon Mine. 24-48 Key Lab 8: 10-1021 <br />Sampling Date: 7/15/20] 0 Wt,,kO7derIV; 0716101002 <br />Sampling Time : Date Received : 07116110 <br />Sample Minn.; Sail Analyse: <br />Sampler: Edward Sample Prep; Total, Open Voss <br />cl <br />Analysis Method : 4CP-MS, EPA Mclb ds 60201200rbp Method: EPA Method 200.8 Opeu Vessel Microwave Diceslion <br /> Wednesday, <br />Date Analyzed: July 21, 2010 <br />23:18:34 Wednesday, <br />July 21, 2010 <br />20:14:39 <br /> Key Loth Prep Batch Sample TD# WI-07208.10- <br />1021-111X10X <br />Sample Comments: <br />Sample Aliquot (mg]: 1081.4 <br />Prep Au Spike Recovery: 1.030 <br />Prop/Digestion DF=» 47.11 <br />Pass Audit==» x Total DF=» 471.08 WI.D7208.10- <br />0000-01 LMB <br />LMB <br />1000 <br />0.983 <br />5o <br />500.00 <br /> L1, Ian <br /> <br />nk L1 Mass Time <br />Symbol <br />m acaA <br />Audit Analyse Reported Value Units <br />tknlr' <br />Methad Blank <br />Blank DF MOL <br />ppm PQL ppm Max QL ppm <br /> I <<= # Analytes Reported <br /> ICRMa• 7 100 L) Lithium mglK9 500.00 0.25 1 500 <br /> tro.MS• s Ia Be Beryllium mg/Kg c < c <br /> I`P-M6' " 10° B Boron mg/Kg 500.00 0.5 2 500 <br /> IC-s• m is Na Sodium mg/Kg < < < <br />kP.Mr ?. to M Magnesium mg/Kg < < < <br />1CP-MS' 21 to Al Aluminum <br />_ mglKg < < c <br />jr,- z° Io FT I Silicon mglKg c < < <br />Icp.1613' 31 10 p Phosphorus mglKg < < < <br />1CP.Ma• 3a IQ K Potassium mg/Kg c < e <br />IcP-Ma• u zo Ca Calcium mg/Kg < c : <br />Icpau• ae to Ti Titanium mg)Kg < e < <br />IcP-Ma• sf 1a V Vaaandium mgtKg < < < <br />KP-Ms' 52 It, Cr 100 Chromium mg/Kg < < < <br />I—.• so Is Mn Man anew mg/Kg - < < < <br />mixus' sr x pe Iron mg/Kg < < < <br />IcP.Ma• ea Io Co Cobalt mglKg < < < <br />epos' 60 ° Ni Nickel mglKg < < < <br />ICPMS• m 1o Cu Copper mgfKg < c < <br />Ic-s• ea Is Zn _ Zinc mg]Kg < < < <br />Knus• 75 too As 100 Arsenic <br />- <br />- mglKg 600.00 0.45 1.8 1D00 <br />Icanls• az 10° Se j <br />0 <br />I x Selenium < mg1Kg < 500.00 0.15 0.fi 1000 <br />ICP.MS• as , w Sr Strontium mglKg 500.00 0.025 0.1 1000 <br />IC-s• go to Mo Molybdenum mglKg e < < <br />tcwas• 107 10 Ag 100 Silver mWKg < < < <br />KP-Ms• 111 t o Cd 20 Cadmium mg/Kg < < < <br />ICPMS• 123 to Sb Antimony mg/Kg < < < <br />KP.MS• 137 tw Ba 2000 Barium mgfKg 600.00 0.03 0.12 1000 <br />w.MS 202 i s H q Mercury mg/Kg < < c <br />-ms- IDS i s TI Thallium mg/Kg < c < <br />ICP-- 30. I o Ph 100 Lead mg/Kg < < < <br />IcP.MS• 227 100 Th Thorium -Wl<g 500.00 0.005 0.02 Soo <br />Kwas• 23a , m U Uranium mg/Kg 500.00 0.005 0.02 500 <br />"Typically, all metals with >=901ms) integration thus can be reported. Available at tusmsan's request, <br />Notes: LMB = laboratory method blank, M and MD • sample matrix replicates <br />Notes: LCS =spiked laboratory method blank, MS and MSD -spiked sample matrix replicates <br />Notes: Au is spiked as sample prep surrogate and to facilitate analysis of Mercury, DF = Dilution Factor, <br />Notes: MDL = Method Detection Limit, POL- PrimaryQuantitatlon Llmlt, MQL= Maximum Quantilation Limit, <br />Notes: < = less than MDL, J = Greater than MDL but less than POL (4 x MDL), E - Estimated Value because It exceeds the MQL <br />Notes: n.a. - Not Applicable, Blank Space = Not Requested or Not Reported <br />Notes: RCRA TCLP Extract Limits: Ba = 100 ppm; [Cr, As,Ag,Pb) = Sppm; [Se, Cd] = 1 ppm; Hg = 0.Z ppm <br />Notes: "(Total RCRA limits) are 20 times the TCLP extract limits because of TCLP sample size (100g) and extract volume (2000mL). <br />"EPA SW946 Method 1311, Revision 0, July 1992, Section 1.2: '4ra total analysis of the waste demonstrates that individual acolytes us not present in the waste, <br /> or that they are present but at such low concentrations that the appropriate regulatory levels could not possibly be exceeded the TCLP need not be con.' <br /> Analyst / Reviewer <br />- ? f