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Key Laboratories, Inc, <br /> Client : Wnlsh Environmental 2479A Riverside Parkway <br /> Client Project Name: New Horizon Mine Grand ]unction, Colorado 81505-1319 <br /> Client Project Number: 009 882.0001.010 Phone (970) 243-5311 Fax (970) 243-6010 <br /> Client Sample Number; TS- 03 <br /> Client Sample Locatian : New Horizon Mine, 0-31 Key Lab k : 10-1013 <br /> Sampling Date : 7/15/2010 Work Order #; 0716101002 <br />Sampling Time: <br />Sample Matrix: Soil Dare Received: <br />Analyst; 07116/10 ffff?111 <br /> <br />LB 1. <br />Sampler: Edward Sample Prep: Total. Open Vessel ` L <br />Analysis Method: •ICP-MS, EPA Methods 6020/201hbp Method: EPA Method200.8 Open Vessel Microwave Oigrstian <br />Wednesday, Wednesday, <br />Date Analyzed: July 21, 2010 July 21, 2010 <br />22:38:27 19:06:20 <br />Key Lab Prep Batch Sample 10H WI-D720A-10- WI-0720A-10. <br />1013.171X1ox D000-01 LMB <br />Sample Comments: LMB <br />Sample Aliquot Itngl: 1006.7 1000 <br />Prep An Spike Recovery: 1.020 01651 <br />Prep/Digestion Dr=>> 49.67 60 . <br />Pass Audit==» x Total Dp=» 496.67 500.00 <br />Analysb 1n Ti- symb.1 acaa <br />uacn? mass Audit Analyte Reported Value Units <br />umlr• <br />Method Blank <br />Blank DF MDL ppm PQL ppm Max QL ppm <br />1 «_= 0 Analytes Reported -1 1 icAMs• 7 109 Li Lithium mg/Kg 500.00 0.25 1 Soo <br /> <br />kP-Ma• 9 19 Be Beryllium mg/Kg c < < <br />ICP-M5• 11 too B Boron mg/Kg 500.00 0.5 2 Soo <br />IOP12 1o Nis Sodium mg/Kg < < < <br />GP-M9• 24 10 M Magnesium mgfKg < < < <br />.clua' 27 10 Al Aluminum mg/Kg < < < <br />ICP-M9• 26 to Si Sfliton mglKg -< < < <br />IcP-MS• 31 to P <br />xP•MS' 99 to r! Phos hotus mgfKg < < < <br /> <br />IcP•MS• u 2a Ca Calcium mg/Kg < < < <br />tcaMS• 4e to Ti Titanium mgfKg < < < <br />ICP-Ma• et m V Vanandium mg/Kg < < < <br />-MS s o Cr 100 Chromium mgfKg e < < <br />icP-Ms' s5 10 Mn Manganese mgfKg < < < <br />Icwts' e4 20 FC Iron mgfKg < < < <br />1M..• s9 10 Co Cobalt m9/Kg < < < <br />' <br />ICP-M9' 60 10 Ni Nickel mgfKg < < < <br />IcP•uc• sa 10 Cu Co per mgfKg < < < <br />rcp-MS' 0 to Zu Zinc mgfKg < c < <br />ICP•Mtt' 75 Inc As 104 Arsenic mg/Kg 500.00 0,45 1.8 1000 <br />' <br />'c ".. ea 10p Se 20 x Selenium < mgfKg < 600.00 0.15 0.6 1000 <br />Icl"MS• 88 100 Sl- Strontium mgfKg 500.00 0.025 0.1 1000 <br />ICP.M5' 09 10 Mo Molybdenum mg/Kg < < <br />< <br />r its' to? 10 Ag 100 Silver mgfKg < < < <br />' <br />,cP-MS• 111 10 Cd 20 Cadmium mgfKg < < < <br />iCP-us• 12s 10 Sb Antimon mgMg < < < <br />I <br />MS• <br />?7 +oo Ba 2000 Barium mgfKg Ismaili 0.03 0.12 1000 <br />MMS <br />zoz <br />ca o Hg 4 Mercury ' mgfKg < < < <br />' <br />rp-Ms. 205 to TI Thallium mg/Kg c < < <br />ICP•Ms' 704 10 Pb 100 Lead mg/Kg < < < <br />WP-M5• 222 109 Th Thorium mgfKg 500.00 0.005 0.02 500 <br />' icp-Ms' 230 1m U 11raniuln m9M9 500.00 O.DO6 0.02 Soo <br />"Typically, all nhetnls with -901nisl integration time nn berePorted. Avmlable at customer's request. <br />Notes: LMB =laboratory method blank, M and MD -sample matrix replicates <br />Notes: LCS - spiked laboratory method blank, MS and MSD - spiked sample matrix replicates <br />' Notes: Au Is spiked as sample prep surrogate and to facilitate analysis or Mercury, DF - Dilution Factor, <br />Notes: MDL - Method Detection Limit, PQL - Primary Quantitation Limit, MQL - Maximum Quantitation Limit, <br />Notes: e - less than MDL, J = Greater than MDL but less than PQL (4 x MDL), E - Estimated Value because It exceeds the M QL <br />Notes: n.a. = Not Applicable, Blank Space - Not Requested or Not Reported <br />Notes: RCRA TCLP Extract Limits: Ba =100 ppm; ICr, As,A9,Pb) - 5ppm; jSe, Cd) - 1 ppm; Ng - 0.2 ppm <br />' <br />Notes: ''(Total RCRA limits) are 20 times the TCLP extract limits because of TCLP sample size (100g) and extract volume (2DOOmL). <br />-EPA SW846 Method 1311, Revision 0. July 1992, Section 1.2: "Ifa total analysis of the waste demonstrates that individual analytes are not Present in th e waste, <br />or that they are present but at such low concentrations that the appropriate regulatory levels could not passbfy be exce deck the TCLP need not be run." <br />Analyst / Reviewer <br />VS