2010-08-18_ENFORCEMENT - C1981008

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Key Laboratories, Inc. Client: Walsh Environmental 2479A Riverside Pwkway Client Project Name: New Horizon Aline Grand Junction, Colorado 81505-1319 Client Project Numb": 900882.0001.010 Phone (970) 243-5311 Fax (970) 243-6010 Client Sample Number: MISS-221A Client Sample Location: New Horizon Kline, 0-24 Key Lab k: 10-1014 Sampling Date: 7115/2010 Work Order k : 0716101002 Sampling Time: Data Received: 07/16/10 t Sample matrix! Soil Analyst: _712 l? Sampler: Edward Sample Prep: Total, Open Vessel Analysis Method : "ICP-MS, EPA Methods 6020 / 20D2p Method EPA Method 200.8 Open Vessel Miemwnve Digesdaa Wednesday, Date Analyzed: July 21, 2010 22:44:15 Wednesday, July 21, 2010 19:05:20 Key Lab Prep Batch Sample IDN W0720A-10- 1014-181X10X Sample Comments: Sample Aliquot Inc& 1090.6 Prep Au Spike Recovery: 1.000 Prep/Digestion DF?> 45.85 Pass Audit ==>> x Total DF=» 458.46 Wi-0720A-10- 0000-01 LMB LMB 1000 0.951 so 500.00 Analy6b ton Tyne RCRA Wmoe Mau m • sy"" umlr• Audit Analyze Reported Value Units Method Blank Blank DF MDL ppm PQL ppm Mex QL ppm I <<== of Analytes Reported ic-w- 7 Boa Li Lithium mgfKg 500.00 0.25 1 600 ICRMS• 6 to Be Beryllium mgfKg < < < Ic0.Ms' It too g Boron mgfKg 500.00 0.5 2 soo IoP.MS' 21 m Na Sodium mgfKg < < < ICRMS' 24 ,o Mg Magnesium mg/Kg < c < IcP.Me' 27 to Al Aluminum mg/Kg < < < IGP-Ms- 28 ,a Si Silicon m91Kg < < < ICP-MS• of to P Phospborns mgfKg < < < Irp-ms. 39 in K Potassium mg/Kg < < < ICp.Ms• M 20 Ca Calcium mgfKg < c < ICRMa' 4a 16 Ti Titanium mgfKg < < < ICRMS• 5t to V Vanandium mg/Kg < < < ICP-Ma' az to Cr 100 Chromium mgfKg < < < ICP.M6' 55 .o Mn Manganese mg/Kg < < < tcP.MS• 64 20 Ize Iron mg/Kg < < < IrA.Ma• s9 to Co Cobalt mg/Kg < < < IcP.MS• w to Ni Nickel mg/Kg < c < ICP-m, ice to Cu CO er mgfKg < < < ICRMS' 66 to Zn Zinc mgfKg < < < ILP.Ms' 15 too AS 100 Arsenic mgfKg 500.00 0.45 1.6 1000 CP.M3• a2 too Se 20 x Selenium < mg/Kg < 500.00 0,15 0.6 1000 ICR116• 66 too Sr Strontium mg/Kg 600.00 0.026 0.1 1000 ILP44- 68 to MO Mol bdenum mgfKg < < < tcP.Ma• tar it, Ag 100 Silver mgfKg < < < GP.MS• tt1 +o Cd 20 Cadmium mg/Kg < < < ILP.MS• 122 to Sb Antimony mgfKg c < < ICP-Ma' 137 too Ba 2000 Barium mgfKg 500.00 0.03 0.12 1000 on-s- 2o2 to Hg A Mercury mgfKg < < < IMP.MS- 2.03 TI Thallium mg/Kg < < < Pb 100 Lead mgfKg 'e < 4 Th Thorium nits g 0.006 0.02 500 roo U Uranium mg11Kg 500,00 0.005 0.02 500 typically, all metals with>=9alms) integration time can be "pot'led. Avauable at customer's request. Notes: LMB = laboratory method blank, M and MD=sample matrix replicates Notes: LCS = spiked laboratory method blank, MS and MSD = spiked sample matrix replicates Notes: Au is spiked as sample prep surrogate and to facilitate analysis of Mercury, DF. Ditution Factor, Notes: MDL= Method Detection Limit, PQL - Primary Quantitation Limit, MOL- Maximum Quarditation Limit, Notes: < = less than MDL, J = Greater then MDL but less than PQL (4 X MDL), E -Estimated Value because It exceeds the MOL Notes: n.a. - Not Applicable, Blank Space - Not Requested or Not Reported Notes: RCRA TCLP Extract Limits: Ba - 100 ppm; [Cr, As,Ag,Pb) = 5ppm; [Se, Cd] - 1 ppm; Hg - 0.2 ppm Notes: "(Total RCRA limits) are 20 times the TCLP extract limits because of TCLP sample size (104g) and extract volume (200DmL). "EPA S W 546 Method 1311, Revision 0, July 1992, Section 1.2: "If a total analysis of the waste demonstrates that individual analyzes are not present in the waste, or iliac they are present but at such low concentrations that the appropriate regulatory levels could not ii-ably be exceeded, the TCLP need not be tun." Analyst/ Reviewer