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<br />Client: Walsh Environmental <br />Client Project Name: New Horizon Mine <br />Client Project Number . 960882.0001.010 <br />Client Sample Number: TS-102 <br />Client Sample Location : New Horizon Mine. 0-24 <br />Sampling Date : 7/1512010 <br />Sampling Time; <br /> <br />Sample Matrix: Soil <br />Sampler: Edward <br />Analysis Method: +ICP-MS, EPA Methods 6020 / 200ti it Method: Key Laboratories, Inc. <br />2479A Riverside Parkway <br />Grand Junction, Colorado 81505-1319 <br />Phone (970) 243-5311 Fax (970) 243-6010 <br /> <br />Key Lab #: 10-1012 <br />Work Order N; 0716101002 <br />Data Received: 07116110 <br />?? ? j?[L <br />Analyst: `7 7 <br />Sample Prep: Total, Open Vessel <br />EPA Method 200.3 Open Vessel Microwave Digestion <br /> Wednesday, <br />Date Analyzed: July 21, 2010 <br />22:32:40 Wednesday, <br />July 21, 2010 <br />19:05:20 <br /> Key Lab Prep Batch Sample 1D8 Wi-0720A-10• <br />1012.161x1ox <br />Sample Comments: <br />Sample Aliquot (mg]: 1065.4 <br />Prep An Spike Recovery: 1.005 <br />Prep/Digestion DF=>> 46.93 <br />Pass Audit =_» x Total DF=» 469.31 WI-0720A-10- <br />uo00-01_LMB <br />LMB <br />1000 <br />0.951 <br />50 <br />$00.00 <br />A"`InI` b" nma srmsel acr:A Audit Analyte Reported Value Units <br />Metapa Ma:: m Llmlr• Method Blank Blank DF MDL ppm PQL ppm Max QL ppm <br /> 1 «__ # Analytes Reported <br />ocpMS• Ito Li Lithium mgfKg 500.00 0.25 1 600 <br />Icp-Ms• a 1. Be Beryllium mg/Kg < < < <br />-.Ma• o 1. B Boron -9/Kg $00.00 0.6 2 goo <br />.1.S' 23 to Na Sodium mgfKg < < < <br />ICRMa• 21 1a Mg Magnesium mg/Kg < < < <br />Icr.Ms• 27 10 Al Aluminum mgfKg < < < <br />1W.Ms• 2e 1o Si Silicon mg1Kg < < < <br />Ic,`Ma' 31 to P Phosphorus mg/Kg < < < <br />ICPMa• 39 to K Potassium mg1Kg < < < <br />I?•1+s' w M Ca Calcium mgfKg < < < <br />ICP•M6• w to Ti Titanium mg/K9 < < < <br />-Ma• a, 10 V Vanandimn mgfKg < < < <br />IGPMa' ea a Cr 100 Chromium mg/Kg < < < <br />ICPM9' SS 10 Mn Manganese mgfKg < < < <br />IGRMa• a1 2e Pe Iron mgfKg e < < <br />tcp.Ms• as to Co Cobalt mgfKg < < < <br />Icp.Ms• w 19 Ni Nickel mgfKg < < < <br />1-.a. r3 1o Cu Copper mgfKg < < < <br />IGP.M6• 66 to Zn Zinc mgfKg < < < <br />Icwsr TO too As 100 Arsenic mgfKg 000.00 0,45 1.9 1000 <br />tcp3ns• at too Se 20 x Selenium < m91K9 < 500.00 0.16 0.6 1000 <br />tc ms- as Ve Sr Strontium mgfKg 500.00 0.025 0.1 1000 <br />IcP.Ms• 9e 10 Me Molybdenum mgfKg < < < <br />tcaMS• 102 1. Ag 100 Silver mgfKg < < < <br />Ie0.MG t„ a Cd 20 Cadmium mgfKg < < < <br />ICPMa' 533 m Sb Antimony mg/Kg < < < <br />IcR- 132 101) Ba 2000 Barium mgfKg 500.00 0.03 0.12 1000 <br />IOP.Ms• m2 is Hg 4 Mercury mg1Kg < < < <br />rp.MS• 206 10 TI Thallium mgfKg < < < <br />roP-MS• 204 to Pb 100 Lead mg/Kg < < < <br />IcP-MS' 232 1w Th Thorium mg1K9 500.00 0.005 0.02 500 <br />IcnMS• 230 100 U Uranium mg/Kg 500.60 0.005 0.02 500 <br /> <br />+Typirnlly, all mdals with>=90[nes( integrnliw, Time em1 he reported. Available et customer's request. <br />Notes: LMB = laboratory method blank, M and MD = sample matrix replicates <br />Notes; LCS - spiked laboratory method blank, MS and MSD= spiked sample matrix replicates <br />Notes: Au is spiked as sample prep surrogate and to facilitate analysis of Mercury, DF = Dilution Factor, <br />Notes: MDL= Method Detection Limit, PCL = PrimaryQuantitation Limit, MQL - Maximum Quantitation Limit, <br />Notes: < e less than MDL, J = Greater than MDL but less than PQL (4 x MDL), E -Estimated Value because It exceeds the MOIL <br />Notes: n.a, - Not Applicable, Blank Space - Not Requested or Not Reported <br />Notes: RCRA TCLP Extract Limits: Da = 100 ppm; [Cr, As,Ag,Pb] = 5ppm; ]Se, Cd] = 1 ppm; Hg - 0.2 ppm <br />Notes: ''(Total RCRA Omits) are 20 times the TCLP extract limits because of TCLP sample size (1008) and extract volume (2000mL). <br />"EPA SW 346 Method 1311, Revision 0, July 1992, Section 1.2: "If a total analysis of the waste demon antes that individual analytes moral present in the waste, <br />or that they are present but at such low concentrations that the appropriate regulatory levels could not possibly be exceeded the TCLP need not be run" <br />Analyst / Reviewer <br />