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Work Order: 08-8652 <br />Client Project ID: <br />ANALYTICAL QC SUMMARY REPORT <br />BatchID: 17234 <br />Sample ID: 084662-01AMS SampType: MS TestCode: 200.713 Run ID: ICP-OPTIMA 5300 DV_081110A Prep Date: 1117/2008 Units: mg/L <br />Client ID: MW-004 Batch ID: 17234 TestNo: E200.7, Rev. FileID: 11100SAM Analysis Date: 1111012008 SegNo: 766894 <br />Analyte Result LQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimft Qual <br />Beryllium <br />Boron <br />Calcium <br />Chromium <br />Cobalt <br />Iron <br />Magnesium <br />Manganese <br />Nickel <br />Potassium <br />Silver <br />Sodium <br />Vanadium <br />Zinc <br />Silicon as Si02(Silica) <br />0.05629 0.000563 <br />2.737 0.0250 <br />333.8 0.484 <br />2.323 0.0125 <br />2.287 0.00625 <br />6.208 0.0875 <br />141.6 0.188 <br />2.578 0.00625 <br />2.285 0.0375 <br />18.88 0.425 <br />0.1797 0.0375 <br />254.1 0.500 <br />2.394 0.0125 <br />2.274 0.0375 <br />29.53 0.134 <br />0.0625 0 90.1 75 125 0 0 <br />2.5 0.2802 98.3 75 125 0 0 <br />12.5 316.1 142 75 125 0 0 <br />2.5 0 92.9 75 125 0 0 <br />2.5 0.003853 91.5 75 125 0 0 <br />6.25 0.07829 99.3 75 125 0 0 <br />12.5 128.5 105 75 125 0 0 <br />2.5 0.265 92.5 75 125 0 0 <br />2.5 0.01285 91.4 75 125 0 0 <br />12.5 6.367 100 75 125 0 0 <br />0.25 0 71.9 75 125 0 0 <br />12.5 246 65 75 125 0 0 <br />2.5 0 95.8 75 125 0 0 <br />2.5 0 91 75 125 0 0 <br />13.38 14.82 110 75 125 0 0 <br />S <br />S <br />S <br />Sample ID: 08-8662-01AMS SampType: MS TestCode: 200.7D Run ID: ICP-OPTIMA 6300 DV 0811106 Prep Date: 11/7/2008 Units: mg/L <br />Client ID: MW-004 Batch ID: 17234 TestNo: E200.7, Rev. FileID: 11100SAM Analysis Date: 11/10/2008 SegNo: 767182 <br />Analyte Result LQL SPKvalue SPK Ref Val %REC LowLimit HighLimit RPD Ref Vai %RPD RPDLimft Qual <br />Lithium 2.549 0.00250 2.5 0.1704 95.1 75 125 0 0 <br />Sample ID: 08-8662-01AMSO SampType: MSD TestCode: 200.713 Run ID: ICP-OPTIMA 6300 DV 081110A Prep Date: 1117/2008 Units: mg/L <br />Client ID: MW-004 Batch ID: 17234 TestNo: E200.7, Rev. FileID: 111008AM Analysis Date: 11/10/2008 SegNo: 766896 <br />Analyte Result LQL SPKvalue SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Aluminum 2.698 0.125 2.5 0.127 103 75 125 2.726 1.03 20 <br />Barium 3.086 0.00250 6.25 0.01643 49.1 75 125 3.082 0.111 20 S <br />Beryllium 0.05604 0.000563 0.0625 0 89.7 75 125 0.05629 0.433 20 <br />Boron 2.725 0.0250 2.5 0.2802 97.8 75 125 2.737 0.440 20 <br />Qualifiers: U - Not detected at or above the Reporting Limit R - RPD outside acceptance limits <br /> J - Analyze detected below quantitation limits B - Analyte detected in the associated Method Blank <br /> S - Spike Recovery outside acceptance limits H - Prep or analytical holding time exceeded <br /> E - Extrapolated value, value exceeds calibration range. X - See case narrative