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033------ <br />Order: 08-8652 <br />Work <br />Client Project ID: <br />ANALYTICAL QC SUMMARY REPORT <br />BatchID: 17234 <br />Sample ID: LCS-17234 SampType: LCS TestCode: 200.7D Run 10: ICP-OPTIMA 5300 DV 081110A Prep Date: 11/712008 Units: mg/L <br /> Batch ID: 17234 TestNo: E200.7, Rev. FileID: 111008AM Analysis Date: 1111012008 SegNo: 766882 <br />Analyte Result LQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Quell <br />Aluminum 2.001 0.100 2 0 100 77.7 113 0 0 <br />Barium 4.937 0.00200 5 0 98.7 80.1 112 0 0 <br />Beryllium 0.04731 0.000450 0.05 0 94.6 75.1 114 0 0 <br />Boron 2.004 0.0200 2 0 100 79 125 0 0 <br />Calcium 9.835 0.387 10 0 98.3 74 113 0 0 <br />Chromium 1.928 0.0100 2 0 96.4 76.2 115 0 0 <br />Cobalt 1.904 0.00500 2 0 95.2 72.1 110 0 0 <br />Iron 4.943 0.0700 5 0 98.9 76.6 115 0 0 <br />Magnesium 9.841 0.150 10 0 98.4 76.7 114 0 0 <br />Manganese 1.9 0.00500 2 0 95 72.4 109 0 0 <br />Nickel 1.901 0.0300 2 0 95.1 69.9 115 0 0 <br />Potassium 9.893 0.340 10 0 98.9 70.9 115 0 0 <br />Silver 0.1568 0.0300 0.2 0 78.4 61 112 0 0 <br />Sodium 9.887 0.400 10 0 98.9 80 120 0 0 <br />Vanadium 1.943 0.0100 2 0 97.1 76.4 112 0 0 <br />Zinc 1.915 0.0300 2 0 95.7 68.5 112 0 0 <br />Silicon as Si02(Silica) 11.03 0.107 10.65 0 104 77.3 115 0 0 <br />Sample ID: LCS-17234 SampType: LCS TestCode: 200.7_D Run ID: ICP-OPTIMA 8300 DV 081110B Prep Date: 1117/2008 Units: mg/L <br /> Batch ID: 17234 TestNo: E200.7, Rev. FileID: 111008AM Analysis Date: 1111012008 SegNo: 767180 <br />Analyte Result LQL SPKvalue SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDUmIt Quell <br />Lithium 1.963 0.00200 2 0 98.1 75 125 0 0 <br />Sample ID: 08.8652-01AMS SampType: MS TestCode: 200.7D Run ID: ICP-OPTIMA 5300 DV 081110A Prep Date: 11/712008 Units: mg/L <br />Client ID: MW-004 Batch ID: 17234 TestNo: E200.7, Rev. FileID: 11100SAM Analysis Date: 11/1012008 SegNo: 766884 <br />Analyte Result LQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimft Qua[ <br />Aluminum 2.726 0.125 2.5 0.127 104 75 125 0 0 <br />Barium 3.082 0.00250 6.25 0.01643 49.1 75 125 0 0 S <br />Qualifiers: U - Not detected at or above the Reporting Limit R - RPD outside acceptance limits <br />J - Analyte detected below quantitation limits B - Analyte detected in the associated Method Blank <br />S - Spike Recovery outside acceptance limits H - Prep or analytical holding time exceeded <br />E - Extrapolated value, value exceeds calibration range. X - See case narrative