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035 <br />Work Order: 08-8652 <br />Client Project ID: <br />ANALYTICAL QC SUMMARY REPORT <br />BatchID: 17234 <br />Sample ID: 08-8652-01AMSD SampType: MSD TestCode: 200.7_D Run ID: ICP-OPTIMA 5300 DV_081110A Prep Date: 11/7/2008 Units: mg/L <br />Client ID: MW-004 Batch ID: 17234 TestNo: E200.7, Rev. FilelD: 11100SAM Analysis Date: 11/10/2008 SegNo: 766895 <br />Analyte Result LQL SPKvalue SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Calcium 327.5 0.484 12.5 316.1 91.5 75 125 333.8 1.91 20 <br />Chromium 2.316 0.0125 2.5 0 92.6 75 125 2.323 0.327 20 <br />Cobalt 2.276 0.00625 2.5 0.003853 91 75 125 2.287 0.509 20 <br />Iron 6.178 0.0875 6.25 0.07829 98.9 75 125 6.208 0.478 20 <br />Magnesium 138.3 0.188 12.5 128.5 78.2 75 125 141.6 2.38 20 <br />Manganese 2.562 0.00625 2.5 0.265 91.9 75 125 2.578 0.644 20 <br />Nickel 2.272 0,0375 2.5 0.01285 90.9 75 125 2.285 0.568 20 <br />Potassium 18.75 0.425 12.5 6367 99.1 75 125 18.88 0.696 20 <br />Silver 0.1818 0.0375 0.25 0 72.7 75 125 0.1797 1.16 20 S <br />Sodium 249.2 0.500 12.5 246 25.7 75 125 254.1 1.96 20 S <br />Vanadium 2.384 0.0125 2.5 0 95.4 75 125 2.394 0.434 20 <br />Zinc 2.258 0.0375 2.5 0 90.3 75 125 2.274 0.729 20 <br />Silicon as Si02(Silica) 29.1 0.134 13.38 14.82 107 75 125 0 0 20 <br />Sample ID: 08.8662-01AMSD SampType: MSD TestCode: 200.7D Run ID: ICP-OPTIMA 6300 DV_081110B Prep Date: 11/712008 Units: mg/L <br />Client ID: MW-004 Batch ID: 17234 TestNo: E200.7, Rev. FilelD: 11100SAM Analysis Date: 11/10/2008 SegNo: 767183 <br />Analyte Result LQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimft Qual <br />Lithium 2.55 0.00250 2.5 0.1704 95.2 75 125 2.549 0.0340 20 <br />QuaNBers: U - Not detected at or above the Reporting Limit R - RPD outside acceptance limits <br />J - Analyte detected below quantitation limits B - Analyte detected in the associated Method Blank <br />S - Spike Recovery outside acceptance limits H - Prep or analytical holding time exceeded <br />E - Extrapolated value, value exceeds calibration range. X - See case narrative