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i~MG~Bj CORE LABORATORIES Q U A L I T Y C O N T R O L R E S U L T S Job Number.: 983261 Report Date.: 12/29/98 CUSTOMER: Greystone PROJECT: OTRY 484-03 Castillo Lnty ATTN: Nick Mathis Test Method........: EPA 200.7 Balch ........ .....: 42373 Analyst...: lmt Method Description.: Metals Analysis(ICAP), Trace Units ........ .....: mg/L Test Code.: FE Parameter..........: Iron (Fe) OC Lab ID Reagen[ OC Resul[ OC Result True Value Orig. Value Lalc. Result ' Limits Date Time LRA 9812080 0.00451 12/16/1998 1126 LRA 981008M 0.00138 12/16/1998 1129 LRA 981203M 9.73337 10.000 12/16/1998 1134 LRA 9810084 0.00153 12/16/1998 1138 LRA 981008K 0.00478 12/16/1998 1142 LRA 981008K 0.00023 12/16/1998 1149 ICV 9812161 5.04189 5.0 100.8 % 90-110 12/16/1998 1153 ICV 981216[ 5.04347 5.0 100.9 X 90-110 12/16/1998 1156 ICB 9812168 -0.00356 0.03 12/16/1998 1202 ISA 980917E 92.08112 99.9075 92.2 % 80-120 12/16/1998 1206 ISB 981120M 91.80241 100.008 91.8 X 80-120 12/16/1998 1210 LCS 980865 76.44950 94.500000 80.9 % 56.8-142.9 12/16/1998 1224 SB 9809295 1.11135 1.00 111.1 % 80-120 12/16/1998 1228 [LV 9812161 5.11649 5.0 102.3 % 90-110 12/16/1998 1256 CCB 9812166 -0.00120 0.03 12/16/1998 1300 PDS 983261-1 9809295 0.98460 1.00 0.00119 98.3 X 75-125 12/16/1998 1332 PSD 983261-1 9809295 0.98709 0.98460 1.00 0.00119 98.6 Y. 75-125 12/16/1998 1335 0.3 R 20 CCU 9812161 5.09225 5.0 101.8 % 90-110 12/16/1998 1340 CCB 9812168 -0.00644 0.03 12/16/1998 1348 SD 983261-1 0.00123 0.00119 12/16/1998 1357 MB 1216 0.01367 0.03 12/16/1998 1415 SB 9809295 1.11614 1.00 111.6 % 80-120 12/16/1998 1419 LL5 980865 102.61776 94.500000 108.6 X 56.8-142.9 12/16/1998 1423 CCV 9812161 4.79719 5.0 95.9 % 90-110 12/16/1998 1540 CCB 9812166 -0.00475 0.03 12/16/1998 1545 CCB 9812168 -0.01406 0.03 12/16/1998 1552 ISA 980917E 88.02954 99.9075 88.1 Y. BO-120 12/16/1998 1628 ISB 981120M 88.62237 100.008 BB.b Y. 80-120 12/16/1998 1632 CCV 9812161 4.79741 5.0 95.9 % 90-110 12/16/1998 1636 CCB 9812166 -0.00096 0.03 12/16/1998 1640 Test Method........: EPA 239.2 Batch .............: 42383 Analyst...: lmt Method Description.: Lead (GFAA) Unfits .............: mg/L Test Code.: PB Parameter..........: Lead (Pb) OC Lab ID Reagent OC Result OC Result True Value Orig. Value Calc. Result * Limits Date Time ICV 981216V 0.04251 0.0400 106.3 % 90-110 12/16/1998 1930 ICB 12168 0.00149 0.002 12/16/1998 1936 SD 983261-1 0.00030 0.00120 12/16/1998 2014 PD5 983261-1 981210H 0.02067 0.020000 0.00120 97.3 % 75-125 12/16/1998 2019 PSD 983261-1 981210H 0.02150 0.02067 0.020000 0.00120 101.5 % 75-125 12/16/1998 2025 3.9 R 20 CCV 981216A 0.05157 0.050000 103.1 Y. 90-110 12/16/1998 2042 CCB 12168 0.00025 0.002 12/16/1998 2048 CCV 981216A 0.05068 0.050000 101.4 % 90-110 12/16/1998 2152 CCB 12168 0.00079 0.002 12/16/1998 2157 CCV 981216A 0.05249 0.050000 105.0 % 90-110 12/16/1998 2250 CCB 12168 0.00112 0.002 12/16/1998 2255 PDS 983153-1 981210R 0.02053 0.020000 0.00094 98.0 Y. 75-125 12/16/1998 2307 PSD 983153-1 981210H 0.02098 0.02053 0.020000 0.00094 100.2 % 75-125 12/16/1998 2313 2.2 R 20 Page 10 * %_% REC, R=RPD, A=ABS Diff., D=% Diff.