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i~~ CORE LABORATORIES Q U A L I T Y C O N T R O L R E S U L T S Job Number.: 983261 Report Date.: 12/29/98 CUSTOMER: Greystone PROJECT: OTRY 484-03 Castillo Ln[y ATTN: Nick Mathis Test Method........ : EPA 239.2 Batch .............: 42383 Analyst...: lmt Method Description. : Lead (GFAA) Uni [s .............: mg/L Test Code.: PB Parameter..........: Lead (Pb) OL Lab ID Reagent QC Result DC Result True Value Orig. Value Calc. Result • Limits Date Time CLV 981216A 0.05449 0.050000 109.0 Y. 90-110 12/16/1998 2359 CCB 12168 0.00108 0.002 12/17/1998 0005 CCV 981216A 0.05191 0.050000 103.8 % 90-110 12/17/1998 0108 CCB 12168 0.00100 0.002 12/17/1998 0114 Test Method........: EPA 200.7 Batch ....... ......: 42373 Analyst...: lmt Method Description.: Metals Analysis(ICAP), Trace Units ....... ......: mg/L Tesi Code.: MN Parameter..........: Manganese (Mn) DC Lab ID Reagent OL Result OC Result True Value Orig. Value Lalc. Result • Limits Date Time LRA 9812080 0.00020 12/16/1998 1126 LRA 98100BM -0.00004 12/16/1998 1129 LRA 981203M 0.00086 12/16/1998 1134 LRA 981008E 1.94355 10.00 12/16/1998 1138 LRA 981008K 0.00022 12/16/1998 1142 LRA 981008K 0.00018 12/16/1998 1149 ICV 9812161 4.75944 5.0 95.2 % 90-110 12/16/1998 1153 I[V 981216E 4.76121 5.0 95.Z Y. 90-110 12/16/1998 1156 ICB 9812166 0.00000 0.001 12/16/1998 1202 I5B 981120M 0.43945 0.5002 87.9 % 80-120 12/16/1998 1210 LCS 980865 1.52239 1.580000 96.4 % 81.0-119.6 12/16/1998 1224 SB 9809295 0.49209 0.50 98.4 X 80-120 12/16/1998 1228 CCV 9812161 4.81546 5.0 96.3 % 90-110 12/16/1998 1256 CCB 9812166 0.00036 0.001 12/16/1998 1300 PDS 983261-1 9809295 0.46801 0.50 0.00035 93.5 % 75-125 12/16/1998 1332 PSD 983261-1 9809295 0.47124 0.46801 0.50 0.00035 94.2 Y. 75-125 12/16/1998 1335 0.7 R 20 CCV 981216E 4.81144 5.0 96.2 Y. 90-110 12/16/1998 1340 LLB 9812166 -0.00001 0-001 12/16/1998 1348 5D 983261-1 0.00007 0.00035 12/16/1998 1357 MB 1216 0.00026 0.001 12/16/1998 1415 SB 9809295 0.52889 0.50 105.8 Y. 80-120 12/16/1998 1419 LLS 980865 1.68944 1.580000 106.9 % 81.0-119.6 12/16/1998 1423 CCV 981216! 4.52753 5.0 90.6 Y. 90-110 12/16/1998 1540 CLB 9812166 0.00002 0.001 12/16/1998 1545 CCB 9812168 -0.00009 0.001 12/16/1998 1552 I5B 981120M 0.42170 0.5002 84.3 % 80-120 12/16/1998 1632 CCV 9812161 4.52917 5.0 90.6 X 90-110 12/16/1998 1636 LCB 9812168 0.00036 0.001 12/16/1998 1640 Test Method........ : EPA 245. 1 earth .............: 42306 Analyst...: veb Method Description. : Mercury (CVAA) Units .............: mg/L Test Code.: HG Parameter.......... : Mercury (Hg) OC Lab ID Reagent OL Result OC Result True Value Orig. Value LaLc. Resin[ ' Limits Dale lime ICV 981111R 0.00406325 0.004000 101.6 % 90-110 12/16/1998 1247 ICB 1216 -0.0000033 0.0002 12/16/1998 1249 CCV 981111M 0.00485700 0.005000 97.1 % 90-110 12/16/1998 1313 CCB 1216 -0.0000027 0.0002 12/16/1998 1315 ' Page 11 ~ " %_% REC, R=RPD, A=ABS Diff., D=% Diff. `Ma ..~.~~..-, ~.•~.~~,A ,.~...ux.,o,~~,c~,rtoo.,,„..,. ~....... _.., .. .,,.~ „~ ..~,.~,r,.,e ,-o~m n.~.cn.~a..o v ~n m,m.nm.,.m ~.. o~~~. ~~.~. ~ .~~,.«.,„~.. ~,,,u~~,~o,.,.