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i~~u~ CORE LABORATORIES D U A L I T Y C O N T R O L R E S U L T S Job Number.: 983261 Report Date.: 12/29/98 CUSTOMER: Greys tone PROJECT: OTRY 464-03 Castillo Cnty A77N: Nick Mathis Test Method........: EPA 200.7 Batch ........... ..: 42373 Analyst...: lmt Method Description.: Metals Anal ysis(ICAP ), Trace Units ........... ..: mg/L Test Code.: CD Parameter..........: Cadmium (Cd) OC Lab ID Reagent OC Result OL Result True Value Orig. Value Lalc. Result + Limits Date Time CCB 9812168 0.00025 0.0006 12/16/1998 1300 PDS 983261-1 9809295 0.04634 0.05 0.00007 92.5 % 75-125 12/16/1998 1332 PSD 983261-1 9809295 0.04683 0.04634 0.05 0.00007 93.5 % 75-125 12/16/1998 1335 1.1 R 20 CCV 9812161 0.96066 1.0 96.1 % 90-110 12/16/1998 1340 CCB 9812168 0.00008 0.0006 12/16/1998 1348 SD 983261-1 0.00014 0.00007 12/16/1998 1357 MB 1216 0.00014 0.0006 12/16/1998 1415 SB 9809295 0.05189 0.05 103.8 Y. BO-120 12/16/1998 1419 LCS 980865 0.37359 0.346000 108.0 % 76.9-123.1 12/16/1998 1423 CCV 9812161 0.92158 1.0 92.2 % 90-110 12/16/1998 1540 LCB 9812168 0.00016 0.0006 12/16/1998 1545 CCB 9812168 0.00012 0.0006 12/16/1998 1552 ISB 981120M 0.86022 0.9985 86.2 X 80-120 12/16/1998 1632 CCV 9812161 0.93399 1.0 93.4 Y. 90-110 12/16/1998 1636 LCB 9812168 0.00009 0.0006 12/16/1998 1640 lest Method........: EPA 200.7 Batch .............: 42373 analyst...: lmt Method Description.: Metals Analysis(ILAP), Trace Units .............: mg/L Tes[ Code.: CR Parameter..........: Chromium (Lr) OC Lab ID Reagent OC Resul[ OC Result True Value Orig. Value Calc. Result • Limits Date Time LRA 9812080 0.00011 12/16/1998 1126 LRA 981008M -0.00055 12/16/1998 1129 LRA 981203M 0.00018 12/16/1998 1134 LRA 981008E 1.95281 10.00 12/16/1998 1138 LRA 981008K 0.00000 12/16/1998 1142 LRA 981008K 0.00019 12/16/1998 1149 ICV 9812161 2.45467 2.5 98.2 Y, 90-110 12/16/1998 1153 ICV 9812161 2.45023 2.5 98.0 X 90-110 12/16/1998 1156 ICB 9812168 -0.00012 0.005 12/16/1998 1202 ISB 981120M 0.44946 0.4993 90.0 % BO-120 12/16/1998 1210 LCS 980865 1.11367 1.080000 103.1 X 73.1-125.9 12/16/1998 1224 SB 9809295 0.20092 0.20 100.5 X 80-120 12/16/1998 1228 CCV 9812161 2.48945 Z.5 99.6 % 90-110 12/16/1998 1256 CCB 9812168 0.00017 0.005 12/16/1998 1300 PDS 983261-1 980929S 0.19059 0.20 0.00004 95.3 % 75-125 12/16/1998 1332 PSD 983261-1 9809295 0.19162 0.19059 0.20 0.00004 95.8 % 75-125 12/16/1998 1335 0.5 R 20 CCV 981216[ 2.47887 2.5 99.2 X 90-110 12/16/1998 1340 LC8 9812168 -0.00009 0.005 12/16/1998 1348 SD 983261-1 0.00012 0.00004 12/16/1998 1357 MB 1216 0.00129 0.005 12/16/1998 1415 SB 9809295 0.21618 0.20 108.1 % 80-120 12/16/1998 1419 LLS 980865 1.25785 1.080000 116.5 % 73.1-125.9 12/16/1998 1423 CCV 9812161 2.33774 2.5 93.5 % 90-110 12/16/1998 1540 CCB 9812168 0.00006 0.005 12/16/1998 1545 CCB 9812168 -0.00002 0.005 12/16/1998 1552 158 981120M 0.43457 0.4993 87.0 % 80-120 12/16/1998 1632 CCV 9812161 2.34087 2.5 93.6 X 90-110 12/16/1998 1636 ccB 9812168 0.00008 0.005 12/16/1998 1640 ~ Page 9 • %=X REC, R=RPD, A=ABS Diff., D=% Diff. ..~. ~~,U.,. .u.. ,aa oc~e~.~~. '"., c~...•.,, ~,., ...,e .. e.. ., ,o.e..,.om„.~,uoe..o.,,,~..o.<.,~an.,`m~„mov^.. o-~., .,.. wr .v ,~.. ,~...,..o