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i~'' CORE LABORATORIES DUAL I T Y C O N T R O L R E S U L T S Job Nunber: 963307 Date: 12/27/96 CUSTOMER: Greystone ~ .. PROJECT: 483-03~ ATTN: Jeff Bpinzig Test Method........: EPA 200.7. ~ ~ ~ Batch .............: 16403 ~ Analyst...: smh Method Descr i~ption. :~ Netals Analysis(ICAP), Trace Reporting Limit...: 0.01 Parameter..... .....: .Copper (CU) ~ Units ......... ....:~ rtg/L OC Lab ID Reagent DC Result OC Result True Value Orig. Value Calc. Result Units Date/Time PDS 963282-1 9611060 0.94622 1.000 0.01203 93.4 X REC 12/11/96 1406 MD 963296-1 0.00028 0.00075 0.00047 ABS Diff. 12111!96 1430 CCV 9610222 2.60167 2.5 104.1 X REC 12/11/96 1441 CCB 9611142 0.00156 12/11/96 1452 PDS 963296-3 9611060 0.94296 1.000 -0.00042 94.3 X REC 12111!96 1500 CCV 9610222 2.61466 2.5 104.6 X REC 12/11/96 1552 CCB 9611142 -0.00047 12/11/96 1607 ISB 960929R 0.40747 0.5000 81.5 X REC 12!11146 1618 CCV 9610222 2.60496 2.5 104.4 X REC 12/11/96 1632 [CB 9611142 -0.00081 12/11/96 1646 CCV 9610222 2.49137 2.5 99.7 X REC 12!11196 2307 CCB 9611142 -0.00067 12/11/96 2320 Test Method........: EPp 200.7 Batch .... .........: 76403 Analyst...: smh Method Description.: Metals Analysis(ICAP), Trace Reporting Limit...: 0.03 Parameter..........: Iron (Fe) Units .............: rt5/L OC Lab ID Reagent OC Result DC Result Tfue Value Orig. Value Ca Lc. Result Units Date/Time ICV 961106Y 2.09366 2.00 104.7 X REC 12/11/96 1018 ICB 9611142 -0.00147 12/11/96 1116 ISA 960929U 160.09834 200 80.0 X REC 12/11/96 1125 ISB 960929R 183.35351 200 91.7 X REC 12/11/96 1135 CCV 9610222 4.97790 5.0 99.6 X REC 12!11/96 1324 CCB 9611142 -0-01132 12/11/96 1339 MD 963282-1 0.00190 0-00417 0.00227 ABS Diff, 12/11/96 1357 PDS 963282-1 9811060 1.85646 2.0000 0.00417 92.6 X REL 12111/46 1406 MD 963296-1 -0.00307 -0.01062 0.00755 ABS Diff. 12/11/96 1430 CCV 9610222 4.98687 5.0 99.7 X REC 12/11/96 1441 CCB 9611142 0.00148 12/11/46 1452 PDS 963296-3 9611060 1.84228 2.0000 -0.02641 93.4 X REC 12/11/96 1500 CCV 9610222 5.17974 5.0 103.6 X REC 12/11/96 1552 CCB 9611142 0.00376 12/11/96 1607 ISA 960929U 162.60217 200 81.3 X REC 12/11/96 1614 158 960929R 196.79466 200 98.4 X REC 12/11/98 1618 CCV 9610222 5.17515 5.0 103.5 X REC 12/11(96 1632 CCB 9611142 -0.00668 12/11/96 1646 CCV 9610222 5.19088 5.0 103.8 X REC 12!11196 1858 [CB 9611142 -0.01671 12/11/96 2007 CCV 9610222 5.08083 5.0 101.6 Y. REC 12/11/96 2128 CCB 9611142 -0.00483 12!11!96 2156 CCV 4610222 5.08735 5.0 101.7 X REC 12/11/96 2307 CCB 9611142 0.00138 12/11/96 2320 CCV 9610222 5.15742 5.0 103.1 X REC 12112!96 0029 CCB 9611142 -0.00069 12/12/96 0042 CCV 9610222 5.10105 5.0 102.0 X REL 12/12/96 0129 CC8 96111LZ 0.00263 12/12/96 0146 ISA 960929U 198.07043 200 99.0 X REC 12/12/96 0208 ISB 960929R 191.55928 200 95.8 X REL 12/12/96 0215 CCV 9610222 4.98014 5.0 99.6 X REC 12/12/96 0225 CCB 9611142 -0.01180 12/12/96 0237 Page 20