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~~l <br />CORE LABORATORIES <br />CI UAL I T Y C O N T R O L R E S U L T S <br />Job Number: 963307 Date: 12!27196 <br />CU550MER: Greystone ~ ~.PROJELT: 483-03 ~ ~ ~~ATTN:. Jeff Spinxig <br />Test Method........: EPA 200.7 ~ ~ ~ BaCCh....~.........; 76403 Malyst...: smh <br />Method Description.: Metals Analysis(LCAP}, Trace. ~ Reporting LimiL..~.:~1.0 <br />Parameter..........: Calci un (Ca) -~~ ~~ ~ Units .............: mg/L <br />OC Lab ID Reagent OC Result OC Result True Value Orig. Value Calc. Result Uni CS Dace/Time <br />CCV <br />CCB 961031A <br />9611142 102.60343 100.00 <br />0.02614 102.6 X REC 12/11196 1625 <br />12/11/96 1646 <br />Test Method........: EPA 200.7 ~ Batch .............: 16403 Analyst...: smh <br />Method Description.: Metals AnaLysis(ICAP), Trace Reporting LimiC...: 0.01 <br />Parameter..........: Chromium (Cr) Units .............: mg/L <br />OC Lab ID Reagent OC ResuL[ OC Result True Value Orig. Value Calc. Result Units Dace/Time <br />ICV 961106Y 2.07622 2.00 103.8 X REG 12/11/96 1018 <br />ICB 9611142 0.00033 12/11/96 1116 <br />ISB 960929R 0.49890 0.5000 99.8 X REL 12/11/96 1135 <br />CCV 9610222 i 2.55263 2.5 102.1 % REC 12!11!96 1324 <br />CCB 9611142 0.00094 12/11/96 1339 <br />MD 963282-1 0.00020 0.00000 0.00020 ABS Diff. 12!11!96 1357 <br />POS 963282-1 9611060 0.96166 1.000 0.00000 96.2 X REL 12/11/96 1406 <br />MD 963296-1 0.00991 0.01005 0.00014 ABS Diff. 12!11796 1430 <br />CCV 9610222 2.55533 2.5 102.2 X REC 12/11/96 1441 <br />CCB 9611142 0.00027 12111196 1452 <br />POS 963296-3 9611060 0.96632 1.000 0.00080 96.6 X REC 12/11/96 1500 <br />CCV 9610222 2.45586 2.5 48.2 X 0.EC 12111196 1552 <br />CCB 9611142 0.00031 12/11/96 1607 <br />ISB 960929R 0.47520 0.5000 95.0 X REC 12/11/96 1618 <br />CCV 9610222 2.48456 2.5 99.4 X REC 12/11/96 1632 <br />CCB 9611142 0.00025 12/11/96 1646 <br />CCV 9610222 2.54491 2.5 101.8 X REC 12/11/96 1858 <br />CCB 9611142 -0.00025 12/11/96 2007 <br />CCV 9610222 2.50670 2.5 100.3 X REC 12/11/96 2128 <br />CCB 9611142 -0.00077 12/11/96 2156 <br />CCV 9610222 2.50107 2.5 100.0 X REL 12/11/96 2307 <br />CCB 9611142 -0.00006 12/11/96 2320 <br />CCV 9610222 2.53400 2.5 101.4 X REC 12!12(96 0029 <br />CCB 9611142 0.00005 12/12/96 0042 <br />CCV 9610222 2.60615 2.5 104.2 X REC 12/12/96 0129 <br />CCB 9611142 -0.00023 12/12/96 0146 <br />ISB 960929R 0.47500 0.5000 95.0 X REC 12/12/96 0215 <br />CCV 9610222 2.56050 2.5 102.4 X REC 12/12/96 0225 <br />CCB 9611142 -0.00000 12112196 0237 <br />Test Method........: EPA 200.7 Batch .....:.......: 16403 Analyst...: smh <br />Method Description.: Metals Analysis(ICAP), Trace Reporting Limit...: 0.01 <br />Parameter..........: Copper (CU) ~ Units .............: mg/L. <br />OC Lab ID Reagen[ OC Result OC Result True Value Orig. Value Catc. Result Units Date/Time <br />lCV 961106Y 2.09083 2.00 104.5 X REC 12/11/96 1018 <br />ICB 9611142 0.00002 12/11/96 1116 <br />ISB 960929R 0.43463 0.5000 86.9 X REC 12/11/96 1135 <br />[CV 9610222 2.61130 2.5 104.5 X REC 12/11/96 1324 <br />CCB 9611142 0.00130 12!11(96 1339 <br />MD 963282-1 0.01216 0.01203 0.00013 ABS Diff. 12/11/96 1357 <br />Page 19 <br />