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WAG~'u' CORE LABORATORIES O U A L[ T Y C O N T R O L R E S U L T S Job Nurber: 963307 Date: 12/27/96 CUSTOMER: Creystone ~ Pt<OJECT:~483-03 ~ ~ ATTNc~~Jeff Spinz ig Test Method........: EPA 200.7 ~ ~~ ~. ~~ ~~ Batch,....:...:....:. 764U3 ~ Analyst...: smh Method Description.: Metals Anal y@is(1 CAP ), Trace Repor Ci nB limit...: '0.01 Parameter..........: Manganese (Mn) ~ ~. ~ ~~ Units .............: mg/L ~: OC Lab ID Reagent OC Result OC Result True Value Orig. Value CaLc. Result Units Date/Time ICV 961106Y 2-04424 2.00 102.2 X REC 12711/46 1018 iL8 9611142 0.00039 12/11/96 1116 ISB 9609290. 0.44796 0-5000 89.6 X REL 12/11/96 1135 CCV 9610222 4.98646 5.0 99.7 X REL 72/11/96 1324 CCB 9611142 0.00088 12/11/96 1339 MD 963282-1 0.00261 0.00274 0.00013 ABS Di ff. 12/11/96 1357 PDS 963282-1 9611060 0.93655 1.000 0.00274 93.4 X REC 12/11/96 1406 MD 963296-1 -0.00195 -0.00194 0.00001 ABS Di ff. 12/11/96 1430 CCV 9670222 5-01438 8.0 100.3 X REC 12/11/96 1441 CCB 9611142 0.00083 12/11196 1452 PDS 963246-3 9611060 9.93730 1-000 -0.00210 93.9 X REC 12/11/96 1500 CLV 9610222 5.17735 5.0 103.5 X REC 12/11/96 1552 tC6 9611142 0.00008 12/11/96 1607 ISB 9609290. 0.45645 0.5000 91.3 X REL 12/11/96 1618 CCV 9610222 5.21989 5.0 104.4 X REC 12711/96 1632 CCB 9611142 0.00052 12/11/96 1646 CCV 9610222 5-17369 5.0 103.5 X REC 12711!96 1858 CCB 9611142 -0.00021 12/11/96 2007 [CV 9610222 5.07586 5.0 101-5 X REC 12/11/96 2128 CCB 9611142 0.00004 12/11/96 2156 CLV 9610222 5.04946 5.0 101.0 X REC 12/11/96 2307 CCB 9611142 0.00032 12/11/96 2320 CCV 9610222 5.10635 5-0 102.1 X REC 12/12/96 0029 CCB 9611142 0.00032 12112!96 0042 CLV 9610222 5-22756 5.0 104.6 X REC 12/12/96 0129 CLB 9611142 0.00008 12/12/96 0146 158 9609290. 0.42885 0.5000 85.7 X REC 12/12/96 0215 CLV 9610222 5.15094 5.0 103.0 X REC 12/12/96 0225 CCB 9611142 -0.00082 12/12/96 0237 T es[ Method........: EPA 200.7 Batch .............: 16403 ~ Analyst...: smh Method Description.: Metals Analysis(tCAP ), Trace ReporCing Limit...: 0.04 Parameter..........: Nickel (Ni) Units .............: mg/L OC Lab ID Reagent OC Result OC Result True Value Orig. Value Lalc. Result Units Date/Time ILV 961106Y 2.06986 2.00 103.5 X REC 12/11/96 1018 ICB 9611142 0.00127 12/11/96 1116 ISB 9609290. 0.93266 1.000 93.3 X REC 12/17/96 1135 CLV 9610222 2.54988 2.5 102.0 X REC 12/11/96 1324 CLB 9611142 0.00013 12/11/96 1339 MD 963282-1 0.00117 0.00092 0.00025 ABS Diff. 12/11/96 1357 PDS 963282-1 9611060 0.91395 1.000 0.00092 91.3 X REC 12/11/96 1406 MD 963296-1 0.00126 0.00067 0.00065 ABS Diff. 12/11/96 1430 CLV 9610222 2.57029 2.5 102.8 X REC 12/11/96 1441 CL8 9611142 0.00179 12(11/96 1452 PDS 963296-3 9611060 0.90155 1.000 0.00112 90.0 X REC 12/11/96 1500 CLV 9610222 2.45009 2.5 98.0 X REC 12111/96 1552 [CB 9611142 0.00121 12/11/96 7607 ISB 9609290. 0.88156 7.000 88.2 X REC 12/11/96 1618 CCV 9610222 2-51469 2.5 100.6 X REL 12/11/96 7632 CCB 9671142 0.00194 12/11/96 7646 Page 21