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~G~ <br />ADDRESS ALL CORRESPONDENCETO: <br />COMMERCIAL TESTING 8 ENGINEERING CO. <br />4665 PARIS STREET, SUITE &200 <br />DENVER, CO 60239 <br />TEL: (303) 373<772 <br />COLORADO -CDPS WET TEST REPORT FORM -CHRONIC FAX: (303)373<791 <br />PERMITTEE: Empire Corporation <br />TYPE TEST: ROUTINE: XX <br />CDPS NO.: CO-0034142 <br />ACCELERATED: <br />OUTFACE: 5d <br />TEST SPECIES: P. promelas <br />TEST RESULTS LETHALITY GROWTH STATISTICAL METHOD <br />Concentration with Statistical Difference 25.0% >100% Dunnett's <br />Pass/Fail Pass N/A <br />IC26PointEstimate >100% >100% Bootstra <br />Pass/Fail Pass N/A <br />TEST TIME & DATE START 1040 AM 06/17/03 END 1135 AM 06/24/03 <br />DILUTION (% EFFLUENT) <br />MEASUREMENTS CONTROL 11.5% 25% 50% 75% 100% <br />Da 1 % Survival 100 100 100 100 100 100 <br />Da 2 97.5 100 100 100 100 100 <br />Da 3 97.5 100 95.0 100 97.5 100 <br />Da 4 97.5 100 95.0 100 97.5 100 <br />Da 5 97.5 97.5 87.5 82.5 90.0 95.0 <br />Da 6 97.5 97.5 77.5 77.5 87.5 92.5 <br />Da 7 97.5 95.0 75.0 75.0 87.5 92.5 <br /> <br />7 Da Mean D Wei ht 0.783 0.871 0.740 0.833 0.813 0.871 <br /> <br />H Maximum/Minimum 8.5/7.8 8.7/8.2 9.0/8.0 9.1/7.9 9.0/7.8 9.1/7.7 <br />RECEIVING WATER USED FOR DILUTION? NO TOTAL RESIDUAL CI" (mg/I): ~.1 <br />HARDNESS (mg/I): REC'V WATER: EFFLUENT: 50 RECON WATER: 123 <br />ALKALINITY (mg/I): REC'V WATER: EFFLUENT: ' 712 RECON WATER: 92 <br />TOTAL AMMONIA tmg/I): INITIAL 100%: <1.0 FINAL 100%: <1.0 <br />WERE ALL TEST CONDITIONS IN CONFORMANCE WITH DIVISION GUIDELINES? YES <br />IF NO, LIST DEVIATIONS FROM TEST SPECIFICATIONS: <br />LABORATORY: SGS COMMERCIAL TESTING & ENGINEERING ANALYST: <br />ccti,_~ - <br />Commercial Testing & Engineering Co. Minerals Services -Corporate Office <br />1919 S. Highland Ave., Suite 1106, Lombard, 7L 60148 t (6 3 01 953-9300 t 16301953"9306 wwwsgs.com <br />I MemOe, W Me SGS Gmu0lSOCKt6 G4nhflf de Survellfnwl <br />F6A5 <br />