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ADDRESS ALL CORRESPONDENCETO: <br />COMMERCIAL TESTING 8 ENGINEERING CO. <br />4865 PARI$ STREET, SUITE 8-200 <br />DENVER, CO 80239 <br />TEL: (303) 373-4772 <br />FAx: (303) 3734791 <br />COLORADO -CDPS WET TEST REPORT FORM -CHRONIC <br />PERMITTEE: Empire Corooration CDPS NO. CO-0034142 OUTFACE: 5d <br />TYPE TEST: ROUTINE: XX <br />ACCELERATED: TEST SPECIES: C. dubia <br />TEST RESULTS LETHALITY REPRODUCTION STATISTICAL METHOD <br />Concentration with Statistical Difference >100% >100% FisherlSteel's Man -One <br />Pass/Fail Pass N/A <br />IC25PointEstimate >100% >100% Bootstra <br />Pass/Fail Pass N/A <br />TEST TIME & DATE START 1115 AM 06/17/03 END 1035 AM 06/25/03 <br />DILUTION (% EFFLUENT) <br />MEASUREMENTS CONTROL 11.5% 25% 50% 75% 100% <br />Da 1 % Survival 100 100 100 100 100 100 <br />Da 2 100 100 100 100 100 100 <br />Da 3 100 100 100 100 100 100 <br />Da 4 100 100 100 100 100 100 <br />Da 5 100 100 100 100 100 100 <br />Da 6 100 100 100 i00 100 100 <br />Da 7 100 100 100 100 100 100 <br /> <br />Mean 3 Brood Total 15.2 11.7 13.0 13.6 11.1 13.0 <br /> <br />H (Maximum/Minimum 8.8/8.2 8.9/8.2 9.0/8.0 9.1/7.9 9,217.8 9.3/7.7 <br />RECEIVING WATER USED FOR DILUTION? NO TOTAL RESIDUAL CI' (mg/I): =r0.1 <br />HARDNESS (mq /f): REC'V WATER: EFFLUENT: 50 RECON WATER: 123 <br /> <br />ALKALINITY (mq /I): REC'1/ WATER: EFFLUENT: ~ 712 RECON WATER: 92 <br />TOTAL AMMONIA (mglp: INITIAL 100%: <1.0 FINAL 100%: <1.0 <br />WERE ALL TEST CONDITIONS IN CONFORMANCE WITH DIVISION GUIDELINES? YES <br />IF NO, LIST DEVIATIONS FROM TEST SPECIFICATIONS: <br />LABORATORY: SGS COMMERCIAL TESTING & ENGINEERING ANALYST: ~__ `,,~ <br />~ Commercial Testing & Engineering Co. I Minerals Services -Corporate Office <br />1919 5. Hi°hland Ave., Suite 2106, Lombard. IL 60148 t (6301953-9300 f (6301953-9306 <br />MamOer of Ne scs Grouy IaociM GenmN as aurveiNencel <br />