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AC3ZI-aboratories, Inc. <br />2773 DownhNl Drive Steamboat Springs, CO 80487 (800) 334-5493 <br />Golder Associates ACZ Project ID: L44806 <br />t - <br />F':F. �� `. t y Lfi'�,/y .-' .. - §5.� °�'�' <br />_ - - - :°` ; r� � _ <br />i w" <br />.rrL;' <br />��i <br />- <br />r'P,A;f+, xr�4�� •' - _ .,�.b-.. l: - <br />L44806-03 NG449751 Bicarbonate as CaCO3 <br />SM2320B - Titration <br />Q6 <br />Sample was received above recommended temperature. <br />WG449740 Calcium. dissolved <br />M200.7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable <br />WG449751 Carbonate as CaCO3 <br />SM2320B - Titration <br />Q6 <br />Sample was received above recommended temperature <br />WG450092 Chloride <br />M300.0 - ion Chromatography <br />Q6 <br />Sample was received above recommended temperature. <br />Q6 <br />M300 0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />M300.0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the concentration of the duplicated <br />sample is too low for accurate evaluation (< 10x MDL). <br />WG449751 Hydroxide as CaCO3 <br />SM2320B - Titration <br />Q6 <br />Sample was received above recommended temperature. <br />pH <br />SM4500H+ B <br />Q6 <br />Sample was received above recommended temperature, <br />pH measured at <br />SM4500H+ B <br />Q6 <br />Sample was received above recommended temperature. <br />W G449609 Residue, Filterable (TDS) @180C <br />SM2540C <br />HC <br />Initial analysis within holding time Reanalysis was past <br />pH measured at <br />SM4500H+ B <br />06 <br />holding time, which was required due to a QC failure during <br />WG449432 <br />Residue, Filterable (TDS) @180C <br />SM2540C <br />the initial analysis. <br />Sample was received above recommended temperature. <br />SM2540C <br />N1 <br />See Case Narrative <br />DC <br />SM2540C <br />Q6 <br />Sample was received above recommended temperature. <br />WG450092 Sulfate <br />M300.0 - Ion Chromatography <br />DC <br />Sample required dilution. Non -target analyte exceeded <br />M300.0 - Ion Chromatography <br />Q6 <br />calibration range <br />WG449751 <br />M300.0 - Ion Chromatography <br />Q6 <br />Sample was received above recommended temperature <br />WG449751 Total Alkalinity <br />SM2320B - Titration <br />Q6 <br />Sample was received above recommended temperature. <br />L44806-04 NG449751 <br />Bicarbonate as CaCC3 <br />SM2320B - Titration <br />Q6 <br />Sample was received above recommended temperature. <br />WG449740 <br />Calcium, dissolved <br />M200.7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG449751 <br />Carbonate as CaCO3 <br />SM2320B - Titration <br />Q6 <br />Sample was received above recommended temperature. <br />WG450092 <br />Chloride <br />M300.0 - Ion Chromatography <br />Q6 <br />Sample was received above recommended temperature <br />M300.0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the concentration of the duplicated <br />sample is too low for accurate evaluation (< 1 O MDL) <br />WG449751 <br />Hydroxide as CaCO3 <br />SM2320B - Titration <br />Q6 <br />Sample was received above recommended temperature. <br />pH <br />SM4500H+ B <br />Q6 <br />Sample was received above recommended temperature <br />pH measured at <br />SM4500H+ B <br />06 <br />Sample was received above recommended temperature. <br />WG449432 <br />Residue, Filterable (TDS) @180C <br />SM2540C <br />Q6 <br />Sample was received above recommended temperature. <br />WG450092 <br />Sulfate <br />M300 0 - Ion Chromatography <br />DC <br />Sample required dilution. Non -target analyte exceeded <br />calibration range. <br />M300.0 - Ion Chromatography <br />Q6 <br />Sample was received above recommended temperature <br />WG449751 <br />Total Alkalinity <br />SM2320B - Titration <br />Q6 <br />Sample was received above recommended temperature <br />REPAD.15.06.05.01 <br />L44806-1807031405 Page 18 of 24 <br />