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AUZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493 <br />Golder Associates ACZ Project ID: L44806 <br />-_-__._--___- <br />�' <br />_"___ _'-s`'__:-'__ <br />'` <br />WG450092 <br />Chloride <br />WG449751 <br />_ <br />L44806-01 NG449603 <br />Bicarbonate as CaCO3 <br />SM2320B - Titration <br />Q6 <br />Sample was received above recommended temperature. <br />W G449740 <br />Calcium, dissolved <br />M200 7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG449603 <br />Carbonate as CaCO3 <br />SM2320B - Titration <br />Q6 <br />Sample was received above recommended temperature. <br />WG450092 <br />Chloride <br />M300.0 - Ion Chromatography <br />DC <br />Sample required dilution. Non -target analyte exceeded <br />calibration range. <br />M300.0 - Ion Chromatography <br />Q6 <br />Sample was received above recommended temperature <br />M300.0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the concentration of the duplicated <br />sample is too low for accurate evaluation (< 10x MDL). <br />WG449603 <br />Hydroxide as CaCO3 <br />SM2320B - Titration <br />Q6 <br />Sample was received above recommended temperature. <br />pH <br />SM4500H+ B <br />Q6 <br />Sample was received above recommended temperature. <br />pH measured at <br />SM4500H+ B <br />Q6 <br />Sample was received above recommended temperature <br />WG449411 <br />Residue, Filterable (TDS) @180C <br />SM2540C <br />Q6 <br />Sample was received above recommended temperature. <br />WG450092 <br />Sulfate <br />M300.0 - Ion Chromatography <br />Q6 <br />Sample was received above recommended temperature. <br />WG449603 <br />Total Alkalinity <br />SM2320B - Titration <br />Q6 <br />Sample was received above recommended temperature <br />L44806-02 NG449751 Bicarbonate as CaCO3 <br />WG449740 Calcium, dissolved <br />WG449751 <br />Carbonate as CaCC3 <br />WG450092 <br />Chloride <br />WG449751 <br />Hydroxide as CaCO3 <br />SM2540C <br />pH <br />pH measured at <br />WG449609 <br />Residue, Filterable (TDS) @180C <br />WG450092 Sulfate <br />WG449751 Total Alkalinity <br />REPAD.15.06.05.01 <br />SM2320B - Titration Q6 <br />M200.7 ICP M3 <br />SM2320B - Titration 06 <br />M300.0 - Ion Chromatography Q6 <br />M300.0 - Ion Chromatography RA <br />SM2320B - Titration <br />Q6 <br />SM4500H+ B <br />Q6 <br />SM4500H+ B <br />Q6 <br />SM2540C <br />HC <br />SM2540C N1 <br />SM2540C Q6 <br />M300.0 - Ion Chromatography DC <br />M300.0 - Ion Chromatography Q6 <br />SM2320B - Titration Q6 <br />Sample was received above recommended temperature <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />Sample was received above recommended temperature. <br />Sample was received above recommended temperature. <br />Relative Percent Difference (RPD) was not used for data <br />validation because the concentration of the duplicated <br />sample is too low for accurate evaluation (< 10x MDL). <br />Sample was received above recommended temperature <br />Sample was received above recommended temperature. <br />Sample was received above recommended temperature <br />Initial analysis within holding time Reanalysis was past <br />holding time, which was required due to a QC failure during <br />the initial analysis <br />See Case Narrative. <br />Sample was received above recommended temperature. <br />Sample required dilution. Non -target analyte exceeded <br />calibration range. <br />Sample was received above recommended temperature. <br />Sample was received above recommended temperature. <br />L44806-1807031405 Page 17 of 24 <br />