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ADZ Laboratories, Inc. <br />2773 Downhill Dnve Steamboat Springs, CO 80487 (800) 334 -5493 <br />Star Mine Operations LLC ACZ Project ID: L16818 <br />ACZ ID WORKNUM PARAMETER <br />METHOD <br />QUAL <br />DESCRIPTION <br />L16818 -03 WG359639 Chloride <br />SM4500CI -E <br />M1 <br />Matrix spike recovery was high, the recovery of the <br />associated control sample (LCS or LFB) was acceptable. <br />SM4500CI -E <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG359571 Cyanide, total <br />M335.4 - Colonmetnc w/ <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />distillation <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL) <br />WG359569 Cyanide, WAD <br />SM4500 -CN I- Colonmetnc w/ <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />distillation <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />WG359747 Fluoride <br />SM450OF -C <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG359297 Phosphorus, ortho dissolved <br />M365.1 - Automated Ascorbic <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />Acid <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL) <br />M365.1 -Automated Ascorbic <br />ZU <br />Analysis date /time preceeds filter date /time. A portion of <br />Acid <br />sample was filtered and analyzed prior to the creation of a <br />Filter workgroup. <br />WG359813 Residue, Filterable (TDS) @180C <br />SM2540C <br />HC <br />Initial analysis within holding time. Reanalysis was past <br />holding time, which was required due to a QC failure during <br />the initial analysis <br />WG359517 Residue, Non - Filterable (TSS) @105C <br />SM2540D <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />L16818 -04 WG359639 Chloride SM4500CI -E <br />SM4500CI -E <br />WG359571 Cyanide, total M335.4 - Colonmetnc w/ <br />distillation <br />WG359569 Cyanide, WAD SM4500 -CN I- Colonmetricw/ <br />distillation <br />WG359747 Fluoride SM450OF -C <br />WG359297 Phosphorus, ortho dissolved M365.1 - Automated Ascorbic <br />Acid <br />M365.1 - Automated Ascorbic <br />Acid <br />WG359517 Residue, Non - Filterable (TSS) @105C SM2540D <br />WG359691 Sulfate D516- 02- Turbidimetric <br />REPAD.15.06.05.01 <br />M1 Matrix spike recovery was high, the recovery of the <br />associated control sample (LCS or LFB) was acceptable. <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL) <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL) <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL) <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />ZU Analysis date /time preceeds filter date /time. A portion of <br />sample was filtered and analyzed prior to the creation of a <br />Filter workgroup. <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />M2 Matrix spike recovery was low, the recovery of the <br />associated control sample (LCS or LFB) was acceptable. <br />L16818- 1402281029 Page 24 of 29 <br />