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ACZ <br />Laboratories, Inc. <br />Steamboat Spnngs, CO 80487 (800) 334 -5493 <br />Star Mine Operations LLC ACZ Project ID: L16818 <br />ACZ ID WORKNUM PARAMETER <br />METHOD <br />L16818 -05 WG359639 Chloride <br />SM4500CI -E <br />M1 <br />Matnx spike recovery was high, the recovery of the <br />associated control sample (LCS or LFB) was acceptable <br />SM4500CI -E <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG359571 Cyanide, total <br />M335 4 - Colonmetnc w/ <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />distillation <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />WG359569 Cyanide, WAD <br />SM4500 -CN I- Colonmetnc w/ <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />distillation <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />WG359747 Fluoride <br />SM450OF -C <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />WG359297 Phosphorus, ortho dissolved <br />M365.1 - Automated Ascorbic <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />Acid <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />M365 1 -Automated Ascorbic <br />ZU <br />Analysis date /time preceeds filter date /time. A portion of <br />Acid <br />sample was filtered and analyzed prior to the creation of a <br />Filter workgroup. <br />WG359517 Residue, Non - Filterable (TSS) @105C <br />SM2540D <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />WG359691 Sulfate <br />D516 -02 - Turbidimetric <br />M2 <br />Matnx spike recovery was low, the recovery of the <br />associated control sample (LCS or LFB) was acceptable. <br />L16818 -06 WG359571 Cyanide, total M335 4 - Colonmetnc w/ RA Relative Percent Difference (RPD) was not used for data <br />distillation validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL) <br />WG359569 Cyanide, WAD SM4500 -CN I- Colormetnc w/ RA Relative Percent Difference (RPD) was not used for data <br />distillation validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />REPAD.15.06.05.01 <br />L16818- 1402281029 Page 25 of 29 <br />