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AraZ Laboratories, Inc. <br />2773 Downhill Dnve Steamboat Spnngs, CO 80487 (800) 334 -5493 <br />Star Mine Operations LLC ACZ Project ID: L16818 <br />ACZ ID WORKNUM PARAMETER <br />METHOD <br />M335.4 - Colonmetric w/ <br />distillation <br />WG359569 <br />Cyanide, WAD <br />L16818 -01 WG359639 Chloride <br />SM4500CI -E <br />M1 <br />Matrix spike recovery was high, the recovery of the <br />WG359297 <br />Phosphorus, ortho dissolved <br />M365.1 - Automated Ascorbic <br />associated control sample (LCS or LFB) was acceptable. <br />SM4500CI -E <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />M365.1 - Automated Ascorbic <br />validation because the sample concentration is too low for <br />WG359813 <br />Residue, Filterable (TDS) @180C <br />SM2540C <br />accurate evaluation (< 1 Ox MDL). <br />WG359461 Cyanide, total <br />M335.4 - Colonmetric w/ <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />distillation <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />WG359569 Cyanide, WAD <br />SM4500 -CN I- Calorimetric w/ <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />distillation <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />WG359297 Phosphorus, oriho dissolved <br />M365.1 - Automated Ascorbic <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />Acid <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />M365.1 - Automated Ascorbic <br />ZU <br />Analysis date /time preceeds filter date /time. A portion of <br />Acid <br />sample was filtered and analyzed prior to the creation of a <br />Filter workgroup <br />WG359813 Residue, Filterable (TDS) @180C <br />SM2540C <br />HC <br />Initial analysis within holding time Reanalysis was past <br />holding time, which was required due to a QC failure during <br />the initial analysis. <br />WG359517 Residue, Non - Filterable (TSS) @105C <br />SM2540D <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 O MDL) <br />L16818 -02 WG359639 Chloride SM4500CI -E <br />SM4500CI -E <br />WG359461 <br />Cyanide, total <br />M335.4 - Colonmetric w/ <br />distillation <br />WG359569 <br />Cyanide, WAD <br />SM4500 -CN I- Colorimetnc w/ <br />distillation <br />WG359297 <br />Phosphorus, ortho dissolved <br />M365.1 - Automated Ascorbic <br />Acid <br />M365.1 - Automated Ascorbic <br />Acid <br />WG359813 <br />Residue, Filterable (TDS) @180C <br />SM2540C <br />WG359517 <br />Residue, Non - Filterable (TSS) @105C <br />SM2540D <br />REPAD.15.06.05.01 <br />M1 Matrix spike recovery was high, the recovery of the <br />associated control sample (LCS or LFB) was acceptable. <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />ZU Analysis date /time preceeds filter date /time. A portion of <br />sample was filtered and analyzed prior to the creation of a <br />Filter workgroup <br />HC Initial analysis within holding time Reanalysis was past <br />holding time, which was required due to a QC failure during <br />the initial analysis. <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />L16818- 1402281029 Page 23 of 29 <br />