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ADZ Laboratories, Inc. <br />Seneca Coal Company ACZ Sample 1D: L11689.O7 <br />Project ID: 451129821 Date Sampled: 04119113 12:45 <br />Sample ID: NPDES3 Date Received: 04119113 <br />Sample Matrix: Surface Water <br />Acidify and filter <br />Colorado 5 CCR 1002- 31.5.31 <br />(Potentially Dissolved) <br />(2009) <br />Total Recoverable <br />M200.2 ICP -MS <br />Digestion <br />ug /L <br />Total Recoverable <br />M200.2 ICP <br />Digestion <br />pmc <br />Metals Analysis <br />ug /L <br />Iron, total recoverable <br />M200.7 ICP <br />Selenium, potentially <br />M200.8 ICP -MS <br />dissolved <br />Selenium, total <br />M200.8 ICP -MS <br />recoverable <br />Wet Chemistry <br />Lab Filtration (glass <br />SOPWC050 <br />fiber filter) <br />khw <br />Residue, Filterable <br />SM25400 <br />(TDS) @1 BOG <br />20 <br />Residue, Non- <br />SM25400 <br />Filterable (TSS) <br />6 mg /L <br />@105C <br />20 <br />04/23/13 15:15 las <br />04/22/13 16:20 las <br />04129/1317:58 jjc <br />0.28 <br />mg /L <br />0.02 <br />0.05 <br />04/30/1312:14 <br />jjc <br />4.9 <br />ug /L <br />0.1 <br />0.3 <br />04/24/13 4:57 <br />pmc <br />4.9 <br />ug /L <br />0.1 <br />0.3 <br />04/24/13 3:53 <br />pmc <br />04122/1311:29 <br />khw <br />1940 <br />mg/L <br />10 <br />20 <br />04/2211313:06 <br />dcw <br />16 <br />6 mg /L <br />5 <br />20 <br />04/2411314:17 <br />dcw <br />REPIN.02.06.05.01 *Please refer to Quallrier Reports for details. <br />Page 8 of 14 <br />