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Laboratories, Inc. <br />Steamboat Springs, CO 80487 <br />Star Mine Operations LLC ACZ Project ID: L12888 <br />AC2:ID WQRKNUfiM PARAMETER METHOD QUAL DESCRIPTION <br />L12888 -03 WG346694 Silica, total M200.7 ICP <br />WG346994 Chloride SM4500CI -E <br />SM4500CI -E <br />WG346890 Cyanide, total M335.4 - Colodmetnc w/ <br />distillation <br />WG346903 Cyanide, WAD SM4500 -CN I- Colorimetricw/ <br />distillation <br />WG346650 Fluoride SM450OF -C <br />WG346196 Phosphorus, ortho dissolved M365.1 - Automated Ascorbic <br />Add <br />M365.1 - Automated Ascorbic <br />Add <br />M365.1 - Automated Ascorbic <br />Add <br />WG346565 Residue, Non•Fikerable (TSS) @105C SM2540D <br />L12938-04 WG346694 Silica, total <br />WG346994 Chloride <br />WG346890 Cyanide, total <br />WG346903 Cyanide, WAD <br />WG346660 Fluoride <br />WG346196 Phosphorus, ortho dissolved <br />M200.71CP <br />SM4500CI -E <br />SM4500CI -E <br />M335.4 - Colorimetric w/ <br />distillation <br />SM4500 -CN I- Colorimetncw/ <br />distillation <br />SM450OF -C <br />M365.1 - Automated Ascorbic <br />Acid <br />M365.1 - Automated Ascorbic <br />Add <br />M365.1 - Automated Ascorbic <br />Add <br />WG346565 Residue, Non•Filterable (TSS) @105C SM2540D <br />REPAD.15.06.05.01 <br />ZS Digestion procedures have the potential to trigger silica <br />polymerization and precipitation, leading to low biased <br />results. Silica chemistry is complex and polymerization <br />kinetics are unpredictable. Dissolved and/or add soluble <br />silica analyses may provide more accurate measurements. <br />M1 Matrix spike recovery was high, the recovery of the <br />associated control sample (LCS or LFB) was acceptable. <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDQ. <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />M2 Matrix spike recovery was low, the recovery of the <br />associated control sample (LCS or LFB) was acceptable. <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />ZU Analysis date/time preceeds filter datettime. A portion of <br />sample was filtered and analyzed prior to the creation of a <br />Filter workgroup. <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />ZS Digestion procedures have the potential to trigger silica <br />polymerization and precipitation, leading to low biased <br />results. Silica chemistry is complex and polymerization <br />kinetics are unpredictable. Dissolved and/or add soluble <br />silica analyses may provide more accurate measurements. <br />Mt Matrix spike recovery was high, the recovery of the <br />associated control sample (LCS or LFB) was acceptable. <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />M2 Matrix spike recovery was low, the recovery of the <br />associated control sample (LCS or LFB) was acceptable. <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />ZU Analysis datettime preceeds filter date/time. A portion of <br />sample was filtered and analyzed prior to the creation of a <br />Filter workgroup. <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />Page 39 of 45 <br />