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AOCZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 <br />Star Mine Operations LLC ACZ Project ID: L12887 <br />REPAD.15.06.05.01 <br />Page 23 of 29 <br />.. <br />L12887 -01 WG346694 Iron, total <br />M200.7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG346886 Molybdenum, dissolved <br />M200.8 ICP -MS <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG346994 Chloride <br />SM4500CI -E <br />M1 <br />Matrix spike recovery was high, the recovery of the <br />associated control sample (LCS or LFB) was acceptable. <br />WG346890 Cyanide, total <br />M335.4 - Colorimetric w/ <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />distillation <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG346875 Cyanide, WAD <br />SM4500 -CN I- Cdorimetric w/ <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />distillation <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG346650 Fluoride <br />SM450OF -C <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG346924 Nltrate/Nrtdte as N <br />M353.2 - H2SO4 preserved <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG346196 Phosphorus, ortho dissolved <br />M365.1 - Automated Ascorbic <br />M2 <br />Matrix spike recovery was low, the recovery of the <br />Add <br />associated control sample (LCS or LFB) was acceptable. <br />M365.1 - Automated Ascorbic <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />Add <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />M365.1 - Automated Ascorbic <br />ZU <br />Analysis datettime preceeds filter date/time. A portion of <br />Add <br />sample was filtered and analyzed prior to the creation of a <br />Filter workgroup. <br />WG346442 Residue, Filterable (TDS) @180C <br />SM2540C <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />WG346439 Residue, Non Filterable (TSS) @105C <br />SM2540D <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />REPAD.15.06.05.01 <br />Page 23 of 29 <br />