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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 <br />Rio Grande Silver, Inc. <br />ACZ ID WORKNUM PARAMETER <br />METHOD QUAL DESCRIPTION <br />REPAD.15.06.05.01 <br />WG330763 Sulfate (1312 DI) <br />D516 -02 - Turbidimetric <br />D516 -02 - Turbidimetric <br />Inorganic Extended <br />Qualifier Report <br />ACZ Project ID: L96798 <br />accurate evaluation (< 10x MDL) <br />HD Analysis is outside the intended scope of the method, <br />which does not provide hold time information for soil <br />extracts No hold time is observed for collection to <br />extraction The referenced method hold time is observed <br />for extraction -to- analysis <br />M1 Matrix spike recovery was high, the recovery of the <br />associated control sample (LCS or LFB) was acceptable <br />Page 27 of 39 <br />