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ENERGY <br />I..! t- }CTIVAI tSl ll! <br />Analyte <br />Method: E200.7 <br />Sample ID: ICV <br />Calcium <br />Iron <br />Magnesium <br />Potassium <br />Sodium <br />Zinc <br />Client: Cotter Corporation <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />www.energylab.com ( Helena, Mr 877 472 - 0711 • Billings, Mr 800 735 - 4489 • Casper, WY 888 235 - 0515 <br />Analytleal &caam.Um.1157 J Gillette, WY 866 -686 -7175 • Rapid City, SD 888- 672 -1225 • College Station, TX 888 -690 -2218 <br />Project: Schwartz SW 10/10/12 S26610 Work Order: C12100556 <br />Method: E200.7 <br />Sample ID: MB -35402 2 Method Blank <br />Iron ND mg /L <br />Zinc 0.003 mg /L <br />QA /QC Summary Report <br />Prepared by Casper, WY Branch <br />Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />Analytical Run ICP2- C_121024B <br />6 Initial Calibration Verification Standard 10/24/12 11:21 <br />51.8 mg /L <br />5.16 mg /L <br />50.2 mg /L <br />47.8 mg /L <br />50.6 mg /L <br />102 mg /L <br />0.50 104 95 105 <br />0.030 103 95 105 <br />0 50 100 95 105 <br />0.50 96 95 105 <br />0.50 101 95 105 <br />0.010 102 95 105 <br />Sample ID: ICSA 6 Interference Check Sample A <br />Calcium 512 mg /L 0.50 102 80 120 <br />Iron 195 mg /L 0.030 98 80 120 <br />Magnesium 520 mg /L 0.50 104 80 120 <br />Potassium 0 00560 mg /L 0.50 <br />Sodium 0.597 mg /L 0.50 <br />Zinc - 0.00640 mg /L 0.010 <br />Sample ID: ICSAB 6 Interference Check Sample AB <br />Calcium 501 mg /L 0.50 100 80 120 <br />Iron 195 mg /L 0.030 98 80 120 <br />Magnesium 496 mg /L 0.50 99 80 120 <br />Potassium 0 000500 mg /L 0.50 <br />Sodium 0.650 mg /L 0.50 <br />Zinc 1.03 mg /L 0.010 103 80 120 <br />0.005 <br />0.002 <br />Run: ICP2-C_121024B <br />Sample ID: LCS3 -35402 2 Laboratory Control Sample Run: ICP2- C_121024B <br />Iron 2.57 mg /L 0.030 103 85 115 <br />Zinc 0.524 mg /L 0.010 104 85 115 <br />Sample ID: C12100556- 001CMS3 2 Sample Matrix Spike Run: ICP2- C_121024B <br />Iron 2.59 mg /L 0.030 103 70 130 <br />Zinc 0.539 mg /L 0.010 105 70 130 <br />Method: E200.7 <br />Sample ID: MB- 121024A 5 Method Blank <br />Calcium ND mg /L 0.06 <br />Iron ND mg /L 0.001 <br />Magnesium ND mg /L 0.03 <br />Potassium ND mg /L 0.06 <br />ND - Not detected at the reporting limit <br />Report Date: 11/08/12 <br />10/24/12 11:50 <br />10/24/12 11:54 <br />Batch: 35402 <br />10/24/12 22:35 <br />10/24/12 22:39 <br />10/24/12 23:40 <br />Sample ID: C12100556- 001CMSD 2 Sample Matrix Spike Duplicate Run: ICP2- C_121024B 10/24/12 23:44 <br />Iron 2.57 mg /L 0.030 102 70 130 0.7 20 <br />Zinc 0 535 mg /L 0.010 104 70 130 0.7 20 <br />Batch: R166285 <br />Run: ICP2-C_121024B 10/24/12 12:14 <br />Page 10 of 25 <br />