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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487(800) 334 -5493 <br />Kerr Coal Company <br />Project ID: <br />Sample ID: <br />Metals Analysis <br />Parameter <br />EPA Method <br />Result Qual XQ Units MDL PQL <br />Date Analyst <br />Calcium, dissolved <br />Iron, dissolved <br />Magnesium, dissolved <br />Manganese, dissolved <br />Potassium, dissolved <br />Sodium, dissolved <br />Wet Chemistry <br />Alkalinity as CaCO3 <br />Bicarbonate as <br />CaCO3 <br />Carbonate as CaCO3 <br />Hydroxide as CaCO3 <br />Total Alkalinity <br />Cation -Anion Balance <br />Cation -Anion Balance <br />Sum of Anions <br />Sum of Cations <br />Chloride <br />Hardness as CaCO3 <br />Lab Filtration <br />Lab Filtration & <br />Acidification <br />Nitrate as N, dissolved <br />Nitrate /Nitrite as N, <br />dissolved <br />Nitrite as N, dissolved <br />Residue, Filterable <br />(TDS) ©180C <br />Sodium Absorption <br />Ratio in Water <br />Sulfate <br />TDS (calculated) <br />TDS (ratio - <br />measured/calculated) <br />REPIN.02.06.05.01 <br />AP -2 <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />56.0 <br />0.10 <br />37.7 <br />0.692 <br />1.9 B <br />31.4 <br />Parameter <br />EPA Method <br />Result Qual XQ Units MIX PQL <br />Date <br />SM2320B - Titration <br />Calculation <br />M325.2 - Colorimetric <br />SM2340B - Calculation <br />SM 3030 B <br />SM 3030 B <br />Calculation: NO3NO2 minus NO2 <br />M353.2 - Automated Cadmium <br />Reduction <br />M353.2 - Automated Cadmium <br />Reduction <br />M160.1 - Gravimetric <br />USGS - 11738 -78 <br />SM4500 SO4 -D <br />Calculation <br />Calculation <br />312 mg /L 2 20 04/25/07 0:00 <br />312 <br />00 <br />7.3 <br />7.3 <br />8 <br />295 <br />40 <br />363 <br />1.07 <br />U <br />U <br />U <br />U <br />U <br />B <br />ACZ Sample ID: <br />Date Sampled: <br />Date Received: <br />Sample Matrix: <br />mg/L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />meq /L <br />meq /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />Inorganic Analytical <br />Results <br />0.2 <br />0.02 <br />0.2 <br />0.005 <br />0.3 <br />0.3 <br />0.1 <br />0.1 <br />1 <br />1 <br />1 <br />0.05 <br />1 <br />0.03 <br />2 <br />2 <br />L62082 -07 <br />04/18/07 08:50 <br />04/18/07 <br />Ground Water <br />04/24/07 21:26 <br />04/25/07 18:16 <br />04/24/07 21:26 <br />04/24/07 21:26 <br />04/24/07 21:26 <br />04/24/07 21:26 <br />2 20 04/25/07 0:00 <br />2 20 04/25/07 0:00 <br />2 20 04/25/07 0:00 <br />0.5 <br />0.5 <br />5 <br />7 <br />04/27/07 0:00 <br />04/27/07 0:00 <br />04/27/07 0:00 <br />04/24/07 13:42 <br />04/27/07 0:00 <br />04/19/07 10:39 <br />04/19/07 12:25 <br />0.80 0.03 0.15 04/27/07 0:00 <br />djt <br />djt <br />djt <br />djt <br />djt <br />djt <br />Analyst <br />I L62082: Page 9 of 17 I <br />wpa <br />wpa <br />wpa <br />wpa <br />calc <br />calc <br />calc <br />jag <br />calc <br />mis <br />mis <br />0.02 0.1 04/27/07 0:00 calc <br />0.02 0.1 04/18/07 21:19 pjb <br />mg /L 0.01 0.05 04/18/07 21:19 pjb <br />390 mg /L 10 20 04/20/07 9:06 Icp <br />calc <br />10 50 04/23/07 9:35 aeh /wpa <br />10 50 04/27/07 0:00 calc <br />04/27/07 0:00 calc <br />Please refer to Qualifier Reports for detail. <br />