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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487(800) 334 -5493 <br />Kerr Coal Company <br />Project ID: <br />Sample ID: <br />Field Data <br />Parameter <br />EPA Method <br />Result Qual XQ Units MDL PQL Date Analyst <br />Conductivity (Field) <br />pH (Field) <br />Temperature (Field) <br />Metals Analysis <br />Parameter <br />EPA Method <br />Result Qual XQ Units MDL PQL <br />Date <br />Calcium, dissolved <br />Iron, dissolved <br />Magnesium, dissolved <br />Manganese, dissolved <br />Potassium, dissolved <br />Sodium, dissolved <br />Wet Chemistry <br />Parameter <br />EPA Method <br />Result Qual XQ Units MDL PQL <br />Date , Analyst <br />Alkalinity as CaCO3 <br />Bicarbonate as <br />CaCO3 <br />Carbonate as CaCO3 <br />Hydroxide as CaCO3 <br />Total Alkalinity <br />Cation -Anion Balance <br />Cation -Anion Balance <br />Sum of Anions <br />Sum of Cations <br />Chloride <br />Hardness as CaCO3 <br />Lab Filtration <br />Lab Filtration & <br />Acidification <br />Nitrate as N, dissolved <br />Nitrate /Nitrite as N, <br />dissolved <br />Nitrite as N, dissolved <br />Residue, Filterable <br />(TDS) @180C <br />Sodium Absorption <br />Ratio in Water <br />Sulfate <br />TDS (calculated) <br />TDS (ratio - <br />measured /calculated ) <br />REPIN.02.06.05.01 <br />AP -2 <br />Field Measurement <br />Field Measurement <br />Field Measurement <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />SM2320B - Titration <br />Calculation <br />325.2 / SM4500CI -E <br />SM2340B - Calculation <br />SM 3030 B <br />SM3030B <br />Calculation: NO3NO2 minus NO2 <br />M353.2 - Automated Cadmium <br />Reduction <br />M353.2 - Automated Cadmium <br />Reduction <br />160.1 / SM2540C <br />USGS -11738-78 <br />SM4500 SO4 -D <br />Calculation <br />Calculation <br />700 <br />7.9 <br />17.0 <br />53.9 <br />0.08 <br />37.3 <br />0.484 <br />2.3 <br />28 8 <br />318 mg /L 2 20 07/14/07 0:00 <br />318 <br />0.0 <br />7.1 <br />71 <br />7 <br />288 <br />0.05 <br />0.05 <br />30 <br />351 <br />1.11 <br />U <br />U <br />* <br />ACZ Sample ID: <br />Date Sampled: <br />Date Received: <br />Sample Matrix: <br />mS /cm <br />units <br />C <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />meq /L <br />meq /L <br />mg /L <br />mg /L <br />8 mg /L <br />B mg /L <br />U ' mg /L <br />B mg /L <br />mg /L <br />Inorganic Analytical <br />Results <br />0.2 <br />0.02 <br />0.2 <br />0.005 <br />0.3 <br />0.3 <br />0.1 <br />0.1 <br />1 <br />1 <br />1 <br />0.05 <br />1 <br />0.03 <br />2 <br />2 <br />0.5 <br />0.5 <br />5 <br />7 <br />L63744-02 <br />07/11/07 13:20 <br />07/11/07 <br />Ground Water <br />07/11/07 13:20 <br />07/11/07 13:20 <br />07/11/07 13:20 <br />07/19/07 22:28 <br />07/19/07 22:28 <br />07/19/07 22:28 <br />07/19/07 22:28 <br />07/21/07 1:30 <br />07/21/07 1:30 <br />2 20 07/14/07 0:00 <br />2 20 07/14/07 0:00 <br />2 20 07/14/07 0:00 <br />08/06/07 0:00 <br />08/06/07 0:00 <br />08/06/07 0:00 <br />07/17/07 9:18 <br />08/06/07 0:00 <br />07/12/07 11 :34 <br />07/12/07 8:47 <br />wfg <br />wfg <br />wfg <br />wfg <br />djt <br />djt <br />calc <br />calc <br />calc <br />amUag <br />calc <br />bjl <br />bjl <br />0.02 0.1 08/06/07 0:00 calc <br />0.02 0.1 07/11/07 21:18 pjb <br />0.01 0.05 07/11/07 21:18 pjb <br />390 mg /L 10 20 07/16/07 15:39 <br />0.74 0.03 0 15 08/06/07 0:00 <br />10 50 07/19/0714:37 <br />10 50 08/06/07 0:00 <br />08/06/07 0:00 <br />* Please refer to Qualifier Reports for detail. <br />L63744: Page 4 of 18 <br />jm <br />jm <br />jm <br />cas <br />cas <br />cas <br />cas <br />aeh <br />calc <br />kmc <br />calc <br />calc <br />