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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 <br />Kerr Coal Company <br />Project ID: <br />Sample ID: <br />Field Data <br />AP -1 1 -2 -3 <br />Parameter EPA Method <br />Result Qual XQ Units MDL PQL <br />Date Analyst <br />Conductivity (Field) <br />pH (Field) <br />Temperature (Field) <br />Metals Analysis <br />Parameter <br />EPA Method <br />Result Qual XQ Units MDL PQL <br />Date <br />Analyst <br />Calcium, dissolved <br />Iron, dissolved <br />Magnesium, dissolved <br />Manganese, dissolved <br />Potassium, dissolved <br />Sodium, dissolved <br />Wet Chemistry <br />Parameter <br />EPA Method <br />Result Qual XQ Units MDL <br />PQL <br />Date Analyst <br />Alkalinity as CaCO3 <br />Bicarbonate as <br />CaCO3 <br />Carbonate as CaCO3 <br />Hydroxide as CaCO3 <br />Total Alkalinity <br />Cation -Anion Balance <br />Cation -Anion Balance <br />Sum of Anions <br />Sum of Cations <br />Chloride <br />Hardness as CaCO3 <br />Lab Filtration <br />Lab Filtration & <br />Acidification <br />Nitrate as N, dissolved <br />Nitrate /Nitrite as N, <br />dissolved <br />Nitrite as N, dissolved <br />Residue, Filterable <br />(TDS) @180C <br />Sodium Absorption <br />Ratio in Water <br />Sulfate <br />TDS (calculated) <br />TDS (ratio - <br />measured/calculated) <br />Field Measurement <br />Field Measurement <br />Field Measurement <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />SM2320B - Titration <br />Calculation <br />SM4500CI -E <br />SM2340B - Calculation <br />SM 3030 B <br />SM 3030 B <br />Calculation: NO3NO2 minus NO2 <br />M353.2 - Automated Cadmium <br />Reduction <br />M353.2 - Automated Cadmium <br />Reduction <br />SM2540C <br />USGS - 11738 -78 <br />SM4500 SO4 -D <br />Calculation <br />Calculation <br />600 <br />8.0 <br />15.0 <br />50.1 <br />0.11 <br />40.2 <br />0.587 <br />0.8 <br />18.7 <br />286 <br />6 <br />291 <br />0.8 <br />6.5 <br />6.6 <br />4 <br />290 <br />B <br />U <br />B <br />* <br />ACZ Sample ID: <br />Date Sampled: <br />Date Received: <br />Sample Matrix: <br />umhos /cm <br />units <br />C <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />meq /L <br />meq /L <br />mg /L <br />mg /L <br />0.2 <br />0.02 <br />0.2 <br />0.005 <br />0.3 <br />0.3 <br />0.1 <br />0.1 <br />1 <br />1 <br />1 <br />0.05 <br />1 <br />0.03 <br />2 <br />2 <br />0.5 <br />0.5 <br />5 <br />7 <br />0.02 B mg /L 0.02 0.1 <br />0.02 B mg /L 0.02 0.1 <br />U * mg /L 0.01 0.05 <br />330 mg /L 10 20 <br />0.48 0.03 0.15 <br />30 <br />322 <br />1.02 <br />B mg /L 10 50 <br />mg /L 10 50 <br />Inorganic Analytical <br />Results <br />L89339 -01 <br />07119111 13:48 <br />07120111 <br />Ground Water <br />07/19/11 13:48 <br />07/19/11 13:48 <br />07/19/11 13:48 <br />07/22/11 20:17 <br />07/22/11 20:17 <br />07/22/11 20:17 <br />07/22/11 20:17 <br />07/22/11 20:17 <br />07/22/11 20:17 <br />2 20 07/22/11 0:00 <br />2 20 07/22/11 0:00 cra <br />2 20 07/22/11 0:00 cra <br />2 20 07/22/11 0:00 cra <br />08/02/11 0:00 <br />08/02/11 0:00 <br />08/02/11 0:00 <br />07/29/11 14:25 <br />08/02/11 0:00 <br />07/21/11 12:35 <br />07/21/11 11:48 <br />07/26/11 11:53 <br />08/02/11 0:00 <br />08/02/11 0:00 <br />jm <br />jm <br />jm <br />aeb <br />aeb <br />aeb <br />aeb <br />aeb <br />aeb <br />cra <br />calc <br />calc <br />calc <br />mpb <br />calc <br />ndm <br />mfm <br />08/02/11 0:00 calc <br />07/20/11 19:37 pjb <br />07/20/11 19:37 pjb <br />07/23/11 11:41 ndm <br />08/02/11 0:00 calc <br />las <br />calc <br />calc <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />Page 2 of 10 <br />