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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 <br />Kerr Coal Company <br />Project ID: <br />Sample ID: <br />Field Data <br />Parameter <br />EPA Method <br />Result Qual XQ Units MDL PQL <br />Date Analyst <br />Conductivity (Field) <br />pH (Field) <br />Temperature (Field) <br />Metals Analysis <br />Parameter <br />EPA Method <br />Result Qual XQ Units MDL PQL <br />Date Analyst <br />Calcium, dissolved <br />Iron, dissolved <br />Magnesium, dissolved <br />Manganese, dissolved <br />Potassium, dissolved <br />Sodium, dissolved <br />Wet Chemistry <br />Parameter <br />EPA Method <br />Result Qua! XQ Units MDL PQL <br />Date Analyst <br />Alkalinity as CaCO3 <br />Bicarbonate as <br />CaCO3 <br />Carbonate as CaCO3 <br />Hydroxide as CaCO3 <br />Total Alkalinity <br />Cation -Anion Balance <br />Cation -Anion Balance <br />Sum of Anions <br />Sum of Cations <br />Chloride <br />Hardness as CaCO3 <br />Lab Filtration (0 45um) <br />& Acidification <br />Lab Filtration (glass <br />fiber filter) <br />Nitrate as N, dissolved <br />Nitrate/Nitrite as N, <br />dissolved <br />Nitrite as N, dissolved <br />Residue, Filterable <br />(TDS) @180C <br />Sodium Absorption <br />Ratio in Water <br />Sulfate <br />TDS (calculated) <br />TDS (ratio - <br />measured/calculated) <br />AP -1 <br />Field Measurement <br />Field Measurement <br />Field Measurement <br />M200.7 ICP <br />M200 7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />SM23208 - Titration <br />Calculation <br />SM4500CI -E <br />SM2340B - Calculation <br />M200 7/200 8 <br />SOPWCO50 <br />Calculation NO3NO2 minus NO2 <br />M353.2 - Automated Cadmium <br />Reduction <br />M353.2 - Automated Cadmium <br />Reduction <br />SM2540C <br />USGS -11738-78 <br />SM4500 SO4 -D <br />Calculation <br />Calculation <br />650 <br />8.0 <br />10.0 <br />47.9 <br />0.11 <br />37 6 <br />0 358 <br />0.9 B <br />18.0 <br />304 mg /L 2 20 10/27/11 0:00 <br />304 <br />-3.8 <br />68 <br />63 <br />5 <br />274 <br />30 <br />322 <br />1.06 <br />U <br />U <br />B <br />umhos/cm <br />units <br />C <br />ACZ Sample ID: <br />Date Sampled: <br />Date Received: <br />Sample Matrix: <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />meq /L <br />meq /L <br />mg /L <br />mg /L <br />B mg /L 10 50 <br />mg /L 10 50 <br />Inorganic Analytical <br />Results <br />0.2 <br />0.02 <br />0.2 <br />0.005 <br />03 <br />0.3 <br />0.1 <br />0.1 <br />1 <br />1 <br />1 <br />0.05 <br />1 <br />0 03 <br />2 <br />2 <br />0.5 <br />05 <br />5 <br />7 <br />L91417 -01 <br />10/19/11 15:30 <br />10/20111 <br />Ground Water <br />10/19/11 15:30 <br />10/19/11 15:30 <br />10/19/11 15:30 <br />10/26/11 10:57 <br />10/26/11 10:57 <br />10/26/11 10:57 <br />10/26/11 10:57 <br />10/26/11 10:57 <br />10/26/11 10:57 <br />2 20 10/27/11 0:00 <br />2 20 10/27/11 0:00 <br />2 20 10/27/11 0:00 <br />10/31/11 11:41 <br />10/31/11 11:41 <br />10/31/11 11:41 <br />10/25/11 15:31 <br />10/31/11 11:41 <br />10/24/11 14:13 <br />jcm <br />jcm <br />jcm <br />aeb <br />aeb <br />aeb <br />aeb <br />aeb <br />aeb <br />cra <br />cra <br />cra <br />cra <br />calc <br />calc <br />calc <br />Ihb <br />calc <br />mfm <br />10/20/11 16:16 las <br />U mg /L 0.02 0.1 10/31/1111.41 calc <br />U mg /L 0.02 0.1 10/20/11 21:44 pjb <br />U * mg /L 0.01 0.05 10/20/11 21 pjb <br />340 mg /L 10 20 10/24/11 16:39 abm <br />0 47 0.03 0 15 10/31/11 11 calc <br />10/24/11 9:02 <br />10/31/11 11:41 <br />10/31/11 11:41 <br />abm <br />calc <br />calc <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />Page 2 of 10 <br />