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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493 <br />Seneca Coal Company <br />Project ID: 450855601 <br />Sample ID: NPDES4 <br />Inorganic Prep <br />= <br />Af'" <br />1 <br />Acidify and filter Colorado 5 CCR 1002-31.5.31 <br />(Potentially Dissolved) (2009) <br />Total Recoverable <br />Digestion <br />Total Recoverable <br />Digestion <br />Metals Analysis <br />#10 <br />Iron, total recoverable <br />Selenium, potentially <br />dissolved <br />Selenium, total <br />recoverable <br />Wet Chemistry <br />REPIN.02.06.05.01 <br />M200.2 ICP-MS <br />M200.2 ICP <br />M200.7 ICP <br />M200.8 ICP-MS <br />M200.8 ICP-MS <br />0.2 <br />5.7 <br />1.3 <br />Lab Filtration (glass SOPWCO50 <br />fiber filter) <br />Residue, Filterable SM2540C <br />(TDS) @180C <br />4440 <br />B <br />mg/L <br />ug/L <br />mg/L <br />ACZ Sample ID: <br />Date Sampled: <br />Date Received: <br />Sample Matrix: <br />0.1 <br />-ct 41;1 <br />0.3 <br />L95063-01 <br />06/11/12 09:30 <br />06/11/12 <br />Surface Water <br />06/13/12 13:24 <br />06/14/12 8:50 mfm <br />06/14/12 20:27 aeb <br />06/15/12 19:02 <br />0.5 1 06/16/12 1:40 <br />06/12/12 11:16 <br />* Please refer to Qualifier Reports for details. <br />mfm <br />aeb <br />pmc <br />ug/L 0.5 1 06/18/12 23:28 pmc <br />mla <br />10 20 06/13/12 15:31 abm <br />Page 2 of 8 <br />