2012-06-28_PERMIT FILE - M2012032 (20)

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AOZ Laboratories, Inc. 2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 Silver Star Resources, LLC L92784-03 WG317138 Manganese, dissolved M200.7 ICP WG317213 Chloride SM4500CI -E WG317289 Cyanide, total M335.4 - Colorimetnc w/ distillation M335.4 - Colorimetric w/ distillation WG317287 Cyanide, WAD SM4500 -CN I- Cdorimetricw/ distillation WG317248 Fluoride SM450OF -C WG317374 Nitrate/Nitrite as N M353.2 - H2SO4 preserved WG316982 Phosphorus, ortho dissolved M365.1 - Automated Ascorbic Add M365.1 - Automated Ascorbic Add WG316967 Residue, Nori-Fifterable (TSS) @105C SM2540D WG317343 Sulfate D516- 02- Turbidimetric L92784.04 WG317138 WG317347 WG317213 WG317289 WG317287 WG317248 WG317374 WG316982 Manganese, dissolved Silver, dissolved Chloride Cyanide, total Cyanide, WAD Fluoride Nitrate/Nitrite as N Phosphorus, ortho dissolved M200.7 ICP M200.8 ICP -MS M200.8 ICP -MS SM4500CI -E M335.4 - Colorimetric w/ distillation M335.4 - Colorimetric w/ distillation SM4500•CN I- Cdorimetricw/ distillation SM450OF -C M353.2 - H2SO4 preserved M365.1 - Automated Ascorbic Add M365.1 - Automated Ascorbic Acid WG316967 Residue, Non- Fifterable (TSS) @105C SM2540D WG317343 Sulfate D516- 02- Turbidimetric REPAD.15.06.05.01 ACZ Project ID: L92784 M2 Matrix spike recovery was low, the recovery of the associated control sample (LCS or LFB) was acceptable. M2 Matrix spike recovery was low, the recovery of the associated control sample (LCS or LFB) was acceptable. M2 Matrix spike recovery was low, the recovery of the associated control sample (LCS or LFB) was acceptable. RA Relative Percent Difference (RPD) was not used for data validation because the sample concentration is too low for accurate evaluation (< 1 Ox MDL). RA Relative Percent Difference (RPD) was not used for data validation because the sample concentration is too low for accurate evaluation (< 1 Ox MDL). RA Relative Percent Difference (RPD) was not used for data validation because the sample concentration is too low for accurate evaluation (< 1 O MDL). RA Relative Percent Difference (RPD) was not used for data validation because the sample concentration is too low for accurate evaluation (< 1 Ox MDL). H3 Sample was received and analyzed past holding time. RA Relative Percent Difference (RPD) was not used for data validation because the sample concentration is too low for accurate evaluation (< 10x MDL). RA Relative Percent Difference (RPD) was not used for data validation because the sample concentration is too low for accurate evaluation (< 1 Ox MDL). M3 The spike recovery value is unusable since the analyte concentration in the sample is disproportionate to the spike level. The recovery of the associated control sample (LCS or LFB) was acceptable. M2 Matrix spike recovery was low, the recovery of the associated control sample (LCS or LFB) was acceptable. M2 Matrix spike recovery was low, the recovery of the associated control sample (LCS or LFB) was acceptable. ZA Poor recovery for Silver quality control is accepted due to low Silver solubility in samples, digestates, or extracts that do not contain sufficient Hydrochloric add. M2 Matrix spike recovery was low, the recovery of the associated control sample (LCS or LFB) was acceptable. M2 Matrix spike recovery was low, the recovery of the associated control sample (LCS or LFB) was acceptable. RA Relative Percent Difference (RPD) was not used for data validation because the sample concentration is too low for accurate evaluation (< IOx MDL). RA Relative Percent Difference (RPD) was not used for data validation because the sample concentration is too low for accurate evaluation (< IOx MDL). RA Relative Percent Difference (RPD) was not used for data validation because the sample concentration is too low for accurate evaluation (< 1 Ox MDL). RA Relative Percent Difference (RPD) was not used for data validation because the sample concentration is too low for accurate evaluation (< 1 Ox MDL). H3 Sample was received and analyzed past holding time. RA Relative Percent Difference (RPD) was not used for data validation because the sample concentration is too low for accurate evaluation (< 1 Ox MDL). RA Relative Percent Difference (RPD) was not used for data validation because the sample concentration is too low for accurate evaluation (< 1 Ox MDL). M3 The spike recovery value is unusable since the analyte concentration in the sample is disproportionate to the spike level. The recovery of the associated control sample (LCS or LFB) was acceptable. Page 29 of 37