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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 <br />St. Sophia Holding Ltd. <br />ACZ ID WORKNUM PARAMETER <br />METHOD <br />QUAL DESCRIPTION <br />L89127 -03 WG306365 Manganese, total <br />REPAD.15.06.05.01 <br />Nickel, total <br />WG306328 Zinc, dissolved <br />WG306490 Chloride <br />WG305302 Chromium, Hexavalent <br />WG305585 Cyanide, total <br />WG306006 Fluoride <br />WG305323 Nitrate /Nitrite as N, dissolved <br />Nitrite as N, dissolved <br />WG306474 Nitrogen, ammonia <br />L89127 -04 WG305585 Cyanide, total <br />M200.8 ICP -MS <br />M200.8 ICP -MS <br />M200.8 ICP -MS <br />SM4500CI -E <br />SM3500Cr -D <br />SM3500Cr -D <br />M335 4 - Colonmetric w/ <br />distillation <br />SM4500F -C <br />M353 2 - Automated Cadmium <br />Reduction <br />M353.2 - Automated Cadmium <br />Reduction <br />M350 1 - Automated Phenate <br />M335.4 - Colonmetric w/ <br />distillation <br />M3 <br />BF <br />M3 <br />RA <br />HE <br />RA <br />RA <br />RA <br />RA <br />RA <br />RA <br />RA <br />Inorganic Extended <br />Qualifier Report <br />ACZ Project ID: L89127 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />Target analyte in prep / method blank at or above the <br />acceptance criteria Target analyte was not detected in the <br />sample 1< MDL]. <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL) <br />Analysis performed past holding time. Method holding time <br />is less than or equal to 7 days and sample was received <br />with less than half of the holding time remaining (refer to <br />item C5 of ACZ's Terms & Conditions). <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL) <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL) <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL) <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />Page 36 of 68 <br />