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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 <br />St. Sophia Holding Ltd. <br />ACZ ID WORKNUM PARAMETER METHOD QUAL DESCRIPTION <br />L89127 -01 WG305853 Total Hot Plate Digestion <br />WG306286 Total Recoverable Digestion <br />WG305358 Biochemical Oxygen Demand (5 day) <br />REPAD.15.06.05.01 <br />M200.2 ICP <br />M200.2 ICP <br />SM5210B <br />Inorganic Extended <br />Qualifier Report <br />ACZ Project ID: L89127 <br />DJ Sample dilution required due to insufficient sample. <br />DJ Sample dilution required due to insufficient sample. <br />HF BOD analysis performed outside of 24 -hour hold time <br />stated in the method but within 48 -hour hold time stated in <br />40 CFR <br />SM5210B K5 The dilution water D.O. depletion was > 0 2 mg/L. <br />WG305522 Chemical Oxygen Demand M410.4 M1 Matrix spike recovery was high, the recovery of the <br />associated control sample (LCS or LFB) was acceptable. <br />M410.4 RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG306490 Chloride SM4500CI -E RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG305302 Chromium, Hexavalent SM3500Cr -D HE Analysis performed past holding time. Method holding time <br />is less than or equal to 7 days and sample was received <br />with less than half of the holding time remaining (refer to <br />item C5 of ACZ's Terms & Conditions). <br />SM3500Cr -D RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG305298 Coliforms, fecal SM9222D - Membrane Filter HE Analysis performed past holding time. Method holding time <br />is less than or equal to 7 days and sample was received <br />with less than half of the holding time remaining (refer to <br />item C5 of ACZ's Terms & Conditions) <br />WG306057 Cyanide, WAD SM4500 -CN I- Colorimetric wl RA Relative Percent Difference (RPD) was not used for data <br />distillation validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG306006 Fluoride SM4500F -C RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG305323 Nitrite as N, dissolved M353.2 - Automated Cadmium RA Relative Percent Difference (RPD) was not used for data <br />Reduction validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL) <br />WG306474 Nitrogen, ammonia M350.1 - Automated Phenate RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG306526 Nitrogen, total Kjeldahl M351.2 - TKN by Block Digester M2 Matrix spike recovery was low, the recovery of the <br />associated control sample (LCS or LFB) was acceptable. <br />M351.2 - TKN by Block Digester RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG305600 Phenol 420.4, Manual Distillation RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL) <br />WG306511 Phosphorus, total M365.1 - Auto Ascorbic Acid RA Relative Percent Difference (RPD) was not used for data <br />(digest) validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG305493 Residue, Non - Filterable (TSS) @105C SM2540D RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG305407 Sulfide as S 376.2 - Methylene Blue RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />Page 34 of 68 <br />