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^11mi4w Laboratories, Inc. <br />2773 Downhill Drive Steamboat Sorinas. CO 80487(800) 334 -5493 <br />Rhino Energy, LLC ACZ Sample ID: L81711 -02 <br />Project ID: Date Sampled: 04119110 12:24 <br />Sample ID: TP -5 SAMPLE 1 Date Received: 04121110 <br />Sample Matrix: Soil <br />Soil Analysis <br />Air Dry at 34 Degrees <br />USDA No. 1, 1972 <br />04/23/10 15:45 <br />me <br />C <br />Parameter <br />EPA Method <br />Result, Qual <br />X0 <br />Units <br />MDL <br />PQL <br />Date <br />Analyst <br />Conductivity @25C <br />SM2510B <br />9.600 <br />* <br />mmhos /cm <br />0.001 <br />0.01 <br />05/05/10 2:57 <br />me <br />pH, Saturated Paste <br />USDA No. 60 (21A) <br />7.8 <br />* <br />units <br />0.1 <br />0.1 <br />05/05/10 2:57 <br />me <br />Saturation Percent <br />USDA No. 60 (2) <br />79.80 <br />% <br />0.01 <br />0.1 <br />05/05/10 2:57 <br />me <br />Sulfur Forms <br />M600/2 -78 -054 3.2.4 -MOD <br />pjb <br />soluble (Water) <br />Reduction <br />Sulfur HCI Residue <br />1.93 <br />% <br />0.01 <br />0.1 <br />05/05/10 0:00 <br />bsu <br />Sulfur HNO3 Residue <br />0.36 <br />* <br />% <br />0.01 <br />0.1 <br />05/05/10 0:00 <br />bsu <br />Sulfur Organic <br />0.36 <br />* <br />% <br />0.01 <br />0.1 <br />05/05/10 0:00 <br />bsu <br />Residual Mod <br />Sulfur Pyritic Sulfide <br />1.57 <br />* <br />% <br />0.01 <br />0.1 <br />05/05/10 0:00 <br />bsu <br />Sulfur Sulfate <br />0.61 <br />% <br />0.01 <br />0.1 <br />05/05/10 0:00 <br />bsu <br />Sulfur Total <br />2.54 <br />* <br />% <br />0.01 <br />0.1 <br />05/05/10 0:00 <br />bsu <br />Total Sulfur minus <br />1.93 <br />* <br />% <br />0.01 <br />0.1 <br />05/05/10 0:00 <br />bsu <br />Sulfate <br />Texture by Hydrometer <br />ASTM D 422 Hydrometer <br />Clay <br />23.8 <br />* <br />% <br />0.1 <br />0.5 <br />04/30/10 0:00 <br />brdlbsu <br />Sand <br />57.5 <br />% <br />0.1 <br />0.5 <br />04/30/10 0:00 <br />brd /bsu <br />Silt <br />18.8 <br />* <br />% <br />0.1 <br />0.5 <br />04/30/10 0:00 <br />brd/bsu <br />Texture Classification <br />Sandy Clay <br />* <br />04/30/10 0:00 <br />brd /bsu <br />Loam <br />Total Solids <br />SM2540B <br />78.70 <br />% <br />0.01 <br />0.1 <br />05/05/10 18:36 <br />me bsu <br />Total Volatile Solids <br />M2540G, Gravimetric <br />56.50 <br />* <br />% <br />0.01 <br />0.1 <br />05/05/10 18:36 <br />me bsu <br />Ll <br />Soil Preparation <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />Page 6 of 20 <br />Air Dry at 34 Degrees <br />USDA No. 1, 1972 <br />04/23/10 15:45 <br />me <br />C <br />Crush and Pulverize <br />USDA No. 1, 1972 <br />04/27/10 17:13 <br />me <br />Digestion - Hot Plate <br />M3050B ICP <br />05/04/10 13:52 <br />bsu <br />Digestion - Hot Plate <br />M3050B ICP -MS <br />05/04/10 13:52 <br />bsu <br />Saturated Paste <br />USDA No. 60 (2) <br />05/03/10 14:24 <br />me <br />Extraction <br />Water Extraction <br />ASA No. 9 10 -2.3.2 <br />05/04/10 9:45 <br />bsu <br />Wet Chemistry <br />:Parameter <br />EPA Method <br />Result Qual XQ Units MDL POL Date Analyst <br />Nitrate /Nitrite as N, <br />M353.2 -Automated Cadmium <br />30.3 mg/Kg 0.3 2 05105/10 23:42 <br />pjb <br />soluble (Water) <br />Reduction <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />Page 6 of 20 <br />