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A-Z Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs. CO 80487 (800) 334 -5493 <br />Rhino Energy, LLC ACZ Sample ID: L81711 -02 <br />Project ID: Date Sampled: 04119110 12:24 <br />Sample ID: TP -5 SAMPLE 1 Date Received: 04121110 <br />Sample Matrix: Soil <br />Metals Analysis <br />:Parameter <br />EPA - .. <br />Qual AQ 1 <br />r <br />Arsenic, total (3050) <br />M6020 ICP -MS <br />8.4 <br />mg/Kg <br />0.3 <br />1 <br />05/06/10 14:18 <br />erf <br />Boron, total (3050) <br />M6010B ICP <br />12 <br />mg/Kg <br />1 <br />5 <br />05/05/10 13:49 <br />ear <br />Cadmium, total (3050) <br />M6020 ICP -MS <br />0.59 <br />mg/Kg <br />0.05 <br />0.3 <br />05/06/10 14:18 <br />erf <br />Calcium, soluble (Sat. <br />M6010B ICP <br />15.10 <br />meq/L <br />0.05 <br />0.2 <br />05/05/10 11:08 <br />aeh <br />Paste) <br />Chromium, total (3050) <br />M6020 ICP -MS <br />82.7 <br />mg/Kg <br />0.3 <br />1 <br />05106/10 14:18 <br />erf <br />Copper, total (3050) <br />M6010B ICP <br />14 <br />mg/Kg <br />1 <br />5 <br />05/05/10 13:49 <br />ear <br />Iron, total (3050) <br />M6010B ICP <br />7500 <br />mg/Kg <br />2 <br />5 <br />05/05/10 13:49 <br />ear <br />Lead, total (3050) <br />M6020 ICP -MS <br />13.70 <br />mg/Kg <br />0.05 <br />0.3 <br />05/06/10 14:18 <br />erf <br />Magnesium, soluble <br />M6010B ICP <br />11.30 <br />meq/L <br />0.08 <br />0.4 <br />05/05110 11:08 <br />aeh <br />(Sat. Paste) <br />Manganese, total <br />M6010B ICP <br />133 <br />mg /Kg <br />0.5 <br />3 <br />05/05/10 13:49 <br />ear <br />(3050) <br />Mercury by Direct <br />M7473 <br />220 <br />ng /g <br />2.41 <br />12.05 <br />04/28/10 20:00 <br />pmc <br />Combustion AA <br />Molybdenum, total <br />M6010B ICP <br />64 <br />mg /Kg <br />1 <br />5 <br />05/05/10 13:49 <br />ear <br />(3050) <br />Selenium, total (3050) <br />M6020 ICP -MS <br />6.47 <br />* mg /Kg <br />0.05 <br />0.3 <br />05/06/10 14:18 <br />erf <br />Sodium Absorption <br />Calculation <br />22.70 <br />0.03 <br />0.15 <br />05/26/10 0:00 <br />talc <br />Ratio <br />Sodium, soluble (Sat. <br />M6010B ICP <br />82.60 <br />meq/L <br />0.09 <br />0.3 <br />05/05/10 11:08 <br />aeh <br />Paste) <br />Zinc, total (3050) <br />M6010B ICP <br />60 <br />mg/Kg <br />1 <br />5 <br />05/05/10 13:49 <br />ear <br />�11 <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />Page 5 of 20 <br />