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Mine Rock Geochemical Analysis <br />Exhibit U — Attachment U -6 <br />• Acid -Base Accounting: A representative sample was ground to 2 mesh and analyzed for <br />pH (1:1 rock: de- ionized water extract), Total Sulfur (high - temperature furnace <br />combustion) a CaCO3 (digestion with hot acid, titration with NaOH). Acid Potential was <br />calculated by multiplying Total Sulfur x 31.25 (Sobek et. al., 1978) and Neutralization <br />Potential calculated from the amount of acid that was neutralized. Acid -Base Potential is <br />calculated from subtracting Acid Potential from Neutralization Potential; and <br />• Synthetic Precipitate Leachate Procedure (SPLP): A representative sample was ground <br />to 21/2 mesh and analyzed in accordance with SW -846 Method 1312 (USEPA, 2007). <br />The leachate was analyzed for metals and trace metals utilizing USEPA Methods 200.7 <br />(Inductively Coupled Plasma- Atomic Emission Spectrometry) and 200.8 (Inductively <br />Coupled Plasma — Mass Spectrometry). The metals analyzed are listed in Exhibit U, <br />Attachment 7, Table U -3. <br />2.0 Analytical Results <br />2.1 Whole Rock Analysis <br />Whole Rock Analytical results are presented in Exhibit U, Attachment 7, Table U -1, and <br />analytical reports are appended to this report. Major elements (reported as oxides) and trace <br />elements (reported as elemental values) comprise 96.9% of the sample. Within the Acid -Base <br />Accounting (Exhibit U, Attachment 7, Table U -2) CaCO3 is reported as 6.2 %, of which 3.1% <br />will be CaCO3 indicating that the majority of the volatile component is CO3' rather than H2O. <br />SiO2 and Al2O3 dominate the oxides, indicating that the sample is felsic in nature, with Ca and K <br />the dominate alkali and alkaline earth metals. Sulfur concentrations as determined by XRF <br />(1.10 %, Exhibit U, Attachment 7, Table U -1) is similar to that determined by combustion <br />(1.75 %, Exhibit U, Attachment 7, Table U -2). Zinc was the dominate trace metal (684 ppm). <br />2.2 Acid -Base Accounting <br />Acid -Base Accounting results are presented in Exhibit U, Attachment 7, Table U -2, and <br />analytical reports are appended to this report. The pH of the mine rock was 7.5. The <br />Neutralizing Potential (62.2 kg /ton) was greater than the Acid Potential (54.6 kg /ton) producing <br />a positive Acid -Base Potential (7.55 kg/ton). <br />2.3 Synthetic Precipitate Leachate Procedure <br />SPLP results are presented in Exhibit U, Attachment 7, Table U -3, and analytical reports are <br />appended to this report. Analytical results were compared to both groundwater and surface <br />water basic standards. For surface water, the chronic standard was used as it was assumed that <br />the leaching of any rock will occur over long periods of time rather than an immediate release. <br />Although the hardness value of the mine rock, based on calculations using the calcium and <br />magnesium concentrations was greater than 400 mg/L as CaCO3, hardness based standards for <br />Wildcat Mining Corporation <br />May Day Idaho Mine Complex — 112d Permit Application <br />Revised August 2011 <br />Exhibit U — Attachment U -6 <br />Page 2 of 3 <br />