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$46 <br />Work Order: 08-1960 <br />Client Project ID: <br />ANALYTICAL QC SUMMARY REPORT <br />BatchID: 15084 <br />Sample ID: 08-1960-01HMS SampType: MS TestCode: 2013.713 Run ID: ICP-OPTIMA 5300 DV_080330A Prep Date: 312712008 Units: mg1L <br />Client ID: MW-002 Batch ID: 15084 TestNo: E200.7, Rev. FilelD: 0328081PM Analysis Date: 312812008 SegNo: 671324 <br />Analyte Result LQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimlt Qual <br />Boron 2.499 0.0250 2.5 0.07487 97 75 125 0 0 <br />Calcium 201.5 0.484 12.5 185.7 127 75 125 C 0 S <br />Chromium 2.304 0.0125 2.5 0 92.2 75 125 C 0 <br />Cobalt 2,234 0.00625 2.5 0 89.3 75 125 0 0 <br />Iron 6.376 0.0875 6.25 0.1157 100 75 125 0 0 <br />Magnesium 65.69 0.188 12.5 52.73 104 75 125 0 0 <br />Manganese 2807 0.00625 2.5 0.5294 91.1 75 125 C 0 <br />Nickel 2236 0.0375 2.5 0 89.4 75 125 0 0 <br />Potassium 17.17 0.425 12.5 4.228 104 75 125 0 0 <br />Sliver 0.2255 0.0375 0.25 D 90.2 75 125 0 0 <br />Sodium 112.6 0.500 12.5 99.3 106 75 125 0 0 <br />Vanadium 2377 0.0125 25 0 95.1 75 125 0 0 <br />Zinc 2.25 0.0375 2.5 0 90 75 125 0 0 <br />Silicon as SM(Silica) 25.32 0.134 13.38 12.57 103 75 125 0 0 <br />Sample ID: 08-1960-01HMS SampType: MS TestCode: 200.713 Run ID: ICP-OPTIMA 5300 DV_020407B Prep Date: 3/27/2008 Units: mg/L <br />Client ID: MW-002 Batch ID: 16084 TestNo: E200.7, Rev. FileID: 040708PM Analysis Date: 41812008 SegNo: 673814 <br />Analyte Result LQL SPKvalue SPKRef Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Lithium 2.495 0,00250 2.5 0.06103 97.4 75 125 0 0 <br />Sample ID: 08-1960.01HMSD SampType: NISD TestCode: 200.713 Run ID: ICP-OPTIMA 5300 OV_080330A Prep Date: 3/27/20DS Units: mg/L <br />Client ID: MW-002 Batch ID: 15084 TestNo: E200.7, Rev. FileID: 032808PM Analysis Date: 3/2812008 SegNo: 671325 <br />Analyte Result LQL SPKvalue SPK Ref Val %REC LowLimit HighLimk RPD Ref Val %RPD RPDLimit Qual <br />Aluminum 2.536 0.125 2.5 0.03257 101 75 125 2.575 1.56 20 <br />Barium 5.903 0,00250 6.25 0,03182 93.9 75 125 6.015 1.69 20 <br />Beryllium 0,05895 0.000563 0,0625 0 94.3 75 125 0.06022 2.13 20 <br />Boron 2.461 0.0250 2.5 0.07487 95.4 75 125 2.499 1.55 20 <br />Calcium 200 0.484 12.5 185.7 115 75 125 201.5 0.745 20 <br />Qualifiers: iJ -Not detected at or above the Reporting Limit R - RPD outside acceptance limits <br /> - Anatyte detected below quantitation limits B - Analyte detected in the associated 4lcthod Blank <br /> S - Spike Recovery outside acceptance limits I I - Prep or analytical holding time exceeded <br /> E - Extrapolated value, value exceeds calibration range. X - See case narrative