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$45 <br />Work Order: 08-1960 <br />Client Project ID: <br />ANALYTICAL QC SUMMARY REPORT <br />BatchID: 15084 <br />Sample ID: LCS-15084 SampType: LCS TestCode: 200.7D Run ID: ICP-OPTIMA 5300 DV_080330A Prep Date: 312712008 Units: mglL <br /> Batch ID: 15084 TestNo: E200.7, Rev. FileID: 032808PM Analysis Date: 312812008 SegNc: 671318 <br />Analyte Result LQL SPK value SPK Ref Val %REC Lowl-lmit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Barium 4.942 0.00200 5 0 98.8 80.1 112 0 0 <br />Beryllium 0.0498 0.000450 0.05 0 99.6 75.1 114 0 0 <br />Boron 1.981 0.0200 2 0 99.1 79 125 0 0 <br />Calcium 10.08 0.387 10 0 101 74 113 0 D <br />Chromium 1.896 0.0100 2 0 94.8 76.2 115 0 0 <br />Cobalt 1.662 0.00500 2 0 93.1 72.1 110 0 0 <br />Iron 5.056 0.0700 5 0 1D1 766 115 0 0 <br />Magnesium 10.17 0,150 10 0 1D2 763 114 0 0 <br />Manganese 1.652 0.00500 2 0 92.6 72.4 109 0 0 <br />Nickel 1.875 0.0300 2 0 93.7 69.9 115 0 0 <br />Potassium 10.28 0.340 10 0.02933 103 70.9 115 0 0 <br />Silver 0.1498 0.0300 0.2 0 74.9 61 112 0 0 <br />Sodium 10.64 0.400 1 D 0.2048 105 80 120 0 0 <br />Vanadium 1.916 0.0100 2 0 95.8 76.4 112 0 0 <br />Zinc 1.888 0.0300 2 0 94.4 68.5 112 0 0 <br />Silicon as Si02(Silica) 10.83 0.107 10.65 0 102 77.3 115 0 0 <br />Sample ID: LCS-15084 SampType: LCS TestCode: 200.713 Run ID: ICP-OPTIMA 5300 DV 0804078 Prep Date: 3/2712008 Units: mglL <br />Batch ID: 15084 TestNo: E200.7, Rev. FIlelC: 04070OPM Analysis Date: 41812008 SegNo: 673812 <br />Analyte Result LQL SPKvalue SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Lithium 1.965 0.00200 2 0 98.3 75 125 0 0 <br />Sample ID: 08.1960-01HMS SampType: MS TestCode: 200.70 Run ID: ICP-OPTIMA 5300 DV 080330A Prep Date: 3/27/2008 Units: mg1L <br />Client ID: MW-002 Batch ID: 15084 TestNo: E200.7, Rev. FileID: 032808PM Analysis Date: 3128/2008 SegNo 671324 <br />Analyte Result LQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Aluminum 2.576 0.125 2.5 0.03257 103 75 125 0 0 <br />Barium 6.015 0.00250 6.25 0.03182 95.7 75 125 0 0 <br />Beryllium 0.06022 0.000563 0.0625 0 96.3 75 125 0 0 <br />Qualifiers: I I - Not detected at or above the Reporting Limit R - RPD outside acceptance limits <br />J - Analyte detected below quantitation limits 8 - Analyte detected in the associated Method Blank <br />S - Spike Recovery outside acceptance limits f I - Prep or analytical holding tune exceeded <br />E - Extrapolated value, value exceeds calibratiexi range. X - See ease narrative