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Key Laboratories, Inc. <br />Client: Walsh Environmental 2479A Riverside Parkway <br />Client Project Name: New Horizon Mine Grand Junction, Colorado 81505.1319 <br />Client Prejeet Number: OQQ 0001.010 Phone (970) 243-5311 Fax (970) 243-6010 <br />Client Sample Number: NHSS-241A <br />Client Sample Location: New Horizon Mine. 0-24 Frey Lab 5: 10-1028 <br />Sampling Date: 7115/2010 Work Order 6: 0716101002 <br />Sampling Time: <br />Sample Matrix: Soil Date Received: <br />Analyst: 07/16110 ???'''''''''??? // }}} <br />V-1 Z? [ t7 <br />Sampler: Edward Sample Prep: Total, Open Vessel <br />Analysis Method: •ICP-MS, EPA Methods 60201200kp Method: EPA Method 200.8 Open Vessel Microwave Digestion <br />Thursday, July Wednesday, <br />Date Analyzed: 22, 2010 July 21, 2010 <br />00:16:64 20:14:38 <br />13:ey Lab Prep Batch Sample tD# WI.0720B-10- WI-a72oB-10- <br />1028-181X1OX 0000-01 LMB <br />Sample Comments: LMB <br />Sample Aliquot [ong[: 1041 1000 <br />Prep Au Spike Recovery: 1.039 0.983 <br />Prep/Digestion DR=» 48.03 60 <br />Pass Audit ae» T..ral nrr-» don 91 cnnen <br /> Ana1y9h Ian In- Sy b., acaA Audit Analyte Reported Value Units Methad Blank Blank DF MDL ppm PQL m Max QL m <br />Me1h9tl Masz s • umtr• PP PP <br /> t «== # Analytes Reported <br /> IcP-us• ' loo Li Lithium m9;K9 500.00 0.25 1 500 <br />ICp-MS• 9 10 Be Beryllium mg/Kg < < < <br />x:paus' " 'm B Boron mg/Kg 500.00 0.6 2 600 <br />ICP-M6• 33 to Na Sodium mg/Kg < < < <br />ICP-MS• 24 to Mg Magnesium mgfKg < < c <br />""s• 27 10 AI Aluminum mg/Kg < < < <br />ICP-Ms• 2e to Si Silicon mglKg < < < <br />101- 31 o p Phosphorus mg/Kg < < c <br />ICP-Ms• 39 to IC Potassium mg1K9 < < < <br />ICP.Mo. 44 20 Ca Calcium mg/Kg < c c <br />61P-Ms• 48 10 Ti Titanium mg/Kg < < < <br />ICP.Aa- 61 10 y Vanandium mg/Kg < < < <br />icy' s2 o Cr 100 Chromium mg/Kg < < c <br />lapMo- 55 ,e Mn Manganese mgfKg < < < <br />ICP-la' sr 20 Fe Iron mgfKg < < < <br />I-- 59 10 Co Cobalt mg/Kg c < < <br />ICPMS 50 to Ni Njckel mg1Kg < e < <br />ICP.Me• 63 to CU Co per mglKg < < < <br />Iw-us• as 19 Zn Zinc mg1Kg c < < <br />xR-MS• rs too As 100 Arsemc mglKg 500.00 0.46 1.8 1000 <br />- a2 10a Se 20 x Selenium 0,24 J mglKg < 500.00 0,16 0.6 1000 <br />ic"s• ae 10o Sr Strontium mg/Kg 600.00 0.026 0.1 1000 <br />IoNma• 96 in MO Molybdenum mglKg < < c <br />lo-s- 107 10 A 100 Silver mg/Kg < < < <br />laves- ,n ut Cd 20 Cadmium mg1Kg < < e <br />1cP-ur 123 10 Sb Antimony mg1Kg < < < <br />ICP.MS• 137 loo Ba 2000 Barium mg/Kg 600.00 0.03 0.12 1000 <br /> 202 Jig 4 ' Mercury mglKg < < < <br />ICRMs• 205 w TI Thallium mg/Kg < < < <br />IC wa- 201 a Pb 100 Lead mglKg < < c <br />?cP-Ma' 232 '°0 Th Thorium mg/Kg 500.00 0.005 0.02 Soo <br />x:p.r . 236 ,w U Uranium mglKg 500.00 0.005 0.02 500 <br /> <br />•.......... ...•••••_••••??•,••--wp,vl c,mae,eponeu. Avnnnomarcusmme-srequeet. <br />Notes: LMB = laboratory method blank, M and MD= sample matrix replicates <br />Notes: LCS = spiked laboratory method blank, MS and MSD = spiked sample matrix replicates <br />Notes: Au Is spiked as sample prep surrogate and to facilitate analysis of Mercury, OF - Dilution Factor, <br />Notes: MDL - Method Detection Limit, PQL - Primary Quantitation Limit, MQL = Maximum Quantitatton Umit, <br />Notes; < - less than MDL, J • Greater than MDL but less than PQL (4 x MDL[, E -Estimated Value because It exceeds the MQL <br />Notes: n.a. = Not Applicable, Blank Space - Not Requested or Not Reported <br />Notes: RCRA TCLP Extract Limits: Ba = 100 ppm; [Cr, As,Ag,Pb[ = 6ppm; [Sa, Cdl = 1 ppm; Hg = 0.2 ppm <br />Notes: ''(Total RCRA limits) are 20 times the TCLP extract limits because of TCLP sample size (100g) and extract volume (2000mL). <br />"EPA SW 346 Method 1311, Revision 0, July 1992. Section 1.2: "Ifs tend analysis of the waste demonstrates that individual analytes are not present in the waste, <br />or that they are present but at such low concentrations that the appropriate regulatory ]"cis could not possibly be exceeded, the TCLP need hot be run. <br />\Analyst / Reviewer <br />V