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Key Laboratories, Inc. <br />Client- Walsh Environmental 2479A Riverside Parkway <br />Client Project Name: New Horizon Mine Grand Junction, Colorado 81505-1319 <br />Client Project Number: 900882.0901.010 Phone (970) 243-5311 Fax (970) 243-6010 <br />Client Sample Number: NHSS-240B <br />Client Sample Location : New Horizon Mine 24-48 hey Lab 0: 10-1027 <br />Sampling Data : 7/H12010 Work Order: 0716101002 <br />Sampling Time : Date Received : 07116110 111 111 <br />Sample Matrix; Soil Analyst: <br />Sampler: Edward Sample Prep: Total, Open Vessel Y tr v'7f l V <br />Analysis Method: -ICP-MS, EPA Methods 6020/2091hp Method: EPA Method 200.8 Open Vessel Microwave Digestion <br /> Thursday, July <br />Date Analyzed: 22, 2010 <br />00:10:11 Wednesday, <br />July 21, 2010 <br />20:14:39 <br /> Key Lab Prep Batch Sample ID9 WI-07208-10- <br />1027.171X10X <br />Sample Comments: <br />Sample Aliquot (mg): 1077.6 <br />Prep Au Spike Recovery: 1.042 <br />Prep/Digestion DF=» 46.40 <br />Pass Audit ==» x Total DF-» 463.99 WI.07206.10- <br />0000.01 LMB <br />LMB <br />1000 <br />0.983 <br />SD <br />500.00 <br /> Anetyab toe rime sva,aet ncaA Audit Ana a Re orted Value Units <br />naeod Mass Ixa' L1.11' <br />P Method Blank Blank DF MDL <br /> <br />PPm PQL ppm Max QL ppm <br /> I «==# Analytes Reported <br /> IcP-MS• 7 'm Li Lithium mgtKg 500.00 0.25 1 500 <br /> ICP.MS- 9 to Be Ber litum mgrKg < < < <br /> I— s' n 1m B Boron mgrKg 500.00 0.6 2 500 <br /> ICNM6' 23 m Na Sodium m91K9 < < < <br /> xcP.MS• 24 to Mg I Magnesium mgrKg < < < <br />rP.MS' v 1o At Aluminum mglKg < < < <br />1e0.1a6• 2D to Si Silicon mg/Kg < < < <br />rcwMr a1 '° p Phosphorus mgrKg c < < <br />-us' 39 10 K Potassium mglKg e < < <br />cPSU• a 20 Ca Calcium mgrKg < < < <br />?P4'^s' 'e 1Q Ti Titanium mg/Kg < < < <br />ac-s• 61 to V Vanandium mg/Kg < < < <br />1-0.W 62 10 Cr 100 Chromium mgrKg < < < <br />!CP-NS "t ,o Mn Manganese mgrKg < < < <br />IcP.MS' m Fe IroO mgrKg < < < <br />ICP.M9• 69 +a Co Cobalt mgXg < < < <br />IcP.MS• fie 1o Ni Nickel mg1Kg < < < <br />nwas• 63 to Cu Copper mg/Kg < < < <br />,.,.Ms- 66 1o Zn Zine mg/Kg < < < <br />I-PAS. 7s +m As 100 Arsenic mg/Kg 600,00 0.45 1.8 1000 <br />KP-NS• 62 too Se 20 x Selenium 0.42 J mgrKg < 500.00 0.15 076 1010 <br />IeP.Ma• ea '°° Sr Strontium mgrKg 500.00 0.026 0.1 1000 <br />x:PNS' W to Mo Molybdenum mgrKg < c < <br />or t6 A 100 Silver mg/Kg c < < <br />, '° Cd 20 Cadmium mgrKg < <br />23 1° Sb Antimony mgrKg <br />37 too Be 2000 Barium mgrKg 600.00 0.03 0.12 1000 <br />07 <br />m 10 HO 4 Mercury mg/Kg <br />6S 10 TI Thallium mgrKg c < < <br />04 ,a Pb 100 Lead mg/Kg < <br />32 1m Th Thorium mgrKg 5 0.02 500 <br />6 <br />2u lw <br />tm U U ranium mgrKg so0.oo o.aos 0.02 Soo <br />' Typically, all metals welt >- 901rnsl integration time can he reported. Available at customer's request. <br />Notes: LMB= laboratory method blank, M and MD - sample matrix replicates <br />Notes: LCS - spiked laboratory method blank, MS and MSD - spiked sample matrix replicates <br />Notes: Au is spiked as sample prep surrogate and to facilitate analysis of Mercury, OF = Dilution Factor, <br />Notes: MDL- Method Detection Limit, PQL -Primary Quantitatlon Limit, MQL= Maximum Quantitation Limit, <br />Notes: <= less than MDL, J = Greaterthan MDL but iess than PQL (4 x MDL), E= Estimated Value because It exceeds the MQL <br />Notes: n.a. = Not Applicable, Blank Space= Not Requested or Not Reported <br />Notes: RCRA TCLP Extract Limits: Ba - 100 ppm; (Cr, As,Ag,Ph] . 5ppm; 1Se, Cd) = 1 ppm; Hg - 0.2 ppm <br />Notes: "(Total RCRA limits) are 20 times the TCLP extract limits because of TCLP sample size (1008) and extract volume (2000mL). <br />"EPA S W846 Method 1311. Revision 0, July 1992, Section 1.2: "If a total analysis of the wane demonstrates that individual analytes are not present in the waste, <br />or that they are present but at such low concentrations that the appropriate regulatory levels could not possibly be exceeded, the TCLP need not be rue" <br />Analyst / Reviewer <br />