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Key Laboratories, Inc. <br />Client: Walsh Environmental 2479A Riverside Parkway <br />Client Project Name: New Horizon Mine Grand Junction, Colorado 81505-1319 <br />Client Project Number : 900882.0001,010 Phone (970) 243-5311 Fax (970) 243-6010 <br />Client Sample Number: TS-95B <br />Client Sample Location: New Horizon Mine, 13-21 Key Lab K: 10-1007 <br />Sampling Date : 7/15/2010 Work Order 9: 0716101002 <br />Sampling Time : <br />Sample Matrix : Soil Date Received : <br />Analyst: 07116/10 ..7 <br />Sampler: Edward Sample Prep: TOW, Open Vessrl LL <br />Analysis Method : '9CP-MS, EPA Methods 6020 / 20Urbp Method: EPA Method 200.8 0pen Vessel Microwave Digestion <br />Wednesday, Wednesday, <br />Date Analyzed: July 21, 2010 July 21, 2010 <br />21;48;48 19:05:20 <br />Key Lab Prep Batch Sample IDM Wi-0720A-10• Wi-0720A-10- <br />1007-111X10X 0000401 LM6 <br />Sample Comments: LMB <br />Sample Aliquot [mg]. 1090.6 1000 <br />Prep Au Spike Recovery: 0.999 0.951 <br />Prep/Digestion DF=» 46.86 s0 <br />Pass Audit ==» x Total DF==>> 468.46 500.00 <br />onarsta loo 1.ma srmaot RO- aa Audit Anal a Reported Value Units <br />Merced Mass u Yt Method Blank Blank DF MDL ppm PQL ppm Max QL ppm <br /> I <-ff Analytes Reported <br />'6P''aa' t ,oo Li Lithium mg/Kg 500.00 0,25 1 Sao <br />tcnMS• 0 10 Be Beryllium n*IKg < < < <br />GPMe' 11 ,m g Boron mgiKg 600.00 0.5 2 Soo <br />a:P MS• n ,e Na Sodium mg/Kg < c < <br />icP-MS• as to M Magnesium mgiKg < < < <br />'cPW zi to Al Aluminum mgiKg c c < <br />IcPa.ts• :e ,o Si Silicon mgfKg < < < <br />tcPMS' al to P Phosphorus mgMg < < < <br />39w KC Potassium mg/Kg <br />0 Ca Calcium mgfKg <br />Ti Titanium mgfKg <br />M <br />V _ Vanandium mgfKg <br />Cr 100 Chromium <br />Mn Man anese mg/Kg <br />Te Iran mgfKg < < < <br />IcNUS• sa o CO Cobalt mgfKg < < < <br />' <br />x.P.Mr m ,o Ni Nickel mgfKg < < < <br />IC0.Me' 83 to Cu Cop er mg/Kg < < < <br />IGN1,15' 66 w Zg Zinc mg/Kg < < < <br />ICRM6' l5 too As 100 Arsenic mgfKg 500.00 0.45 1.8 1000 <br />rcPMS• at ,w Se 20 x SClenium 0.26 J mgfKg a 500.00 0,15 0.8 1000 <br />Icaps• ee +m Si- Strontium mgfKg 500.00 0.025 0.1 1000 <br />IcP.Mr m to Mo Molybdenum mg/Kg < < < <br />xrMS• tot +o A 100 Silver mg/Kg < < < <br />tcP•MS• u+ ,o Cd 20 Cadmium mgiKg < < < <br />ICP-MS• lA +o Sb Antimony mg/Kg < < < <br />' ,ar too Ba 2000 Barium mg/Kg 500.00 0.01 0.12 1000 <br />Ic -Ms• 2o2 ,o H 4 Mercury mg/Kg < < < <br />mp-MS' '05 w TI Thallium mgiKg < < < <br />-.a. 1es to Pb 100 Lead mg/Kg < < < <br />teP-MS 2U too Th Thorium mg/Kg 600.00 0.005 0.02 500 <br />Icr-Me• za6 too U Uranium mg/Kg 500.00 0.005 0.02 500 <br />_ <br />a 'Typiullly, allmetals wlth>=901mslintegrntiutstiniecmbereparted. AvaOableateustomer'srequest. <br />t.? <br />Notes: LIVID = laboratory method blank, M and MD= sample matrix replicates <br />_ Notes: LCS = spiked laboratory method blank, MS and MSD = spiked sample matrix replicates <br />Notes: Au Is spiked as sample prep surrogate and to facilitate analysis of Mercury, DF = Dilution Factor, <br />Notes: MOL - Method Detection Limit. PQL =Primary Quantitation Limit, MQL= Maximum QuanUtation Limit, <br />Notes; <= less than MDL, J = Greaterthan MDL but less than PQL (4 x MOL), E= Estimated Value because it exceeds the MQL <br />Notes: n.a. = Not Applicable, Blank Space - Not Requested or Not Reported <br />- Notes: RCRA TCLP Extract Limits: Ba = 100 ppm; ICr, As,Ag,Pbj - Sppm; [Se, Cd]= 1 ppm; Hg = 0.2 ppm <br />Notes: -(Totar RCRA limits) are 20 times the TCLP extract limits because of TCLP sample size (1008) and extract volume (20DOmL), <br />-EPA S W 846 Method 1311. Revision O, July 1992, Seuion 1.2: "If a total analysis of the waste demonstrates that individual analytes are not present in the waste, <br />or that they are present but at such low cenceatration, that the appropriate regulatory levels could not possibly be exceeded, the TCLP need not be run" <br />Analyst / Reviewer <br />