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Key Laboratories, Inc. <br />Client: Walsh Environmental 2479A Riverside Parkway <br />Client Project Name: New Hgrizan Mine Grand Junction, Colorado 81505-1319 <br />Client Project Number : 900882.0001.010 Phone (970) 243-5311 Fax (970) 243-60 10 <br />Client Sample Number; TS-95A <br />Client Sample Location ; New Horizon Mine, 0-13 Key tab 4: 10-1006 <br />Sampling Date : 7/1512010 Work Order a : 0716101002 <br />Sampeiime: Dote Received: 07116/10 <br />Sample Matrix: Soil {t <br />Analyst: \V/vJ\/ '7_'?^y <br />Sampler-, Edward r <br />Sample Prep: Talxt, Open Vessel <br />Analysis Medved: ^ICP-MS, EPA Methods 60201209itp Method: EPA Method 200.8 Open Vessel Microwave Digestion <br />' Date Analyzed; July 21, 2010 July 21, 2010 <br /> 21:41:07 19:05:20 <br />Key Lab Prep Batch Sample IDk Wt-0720A"10- Wt-0720A-10. <br /> 1006-101X10X 0000-01_LMB <br />Sample Comments: LMB <br />Sample Aliquot lmgl: 1047.6 1000 <br />Prep Au Spike Recovery; 1.016 0.961 <br />Prep/Digestion DF=->> <br />Pas<Audit ==55 T.,a.,t nc-- 47.73 <br />--1P 60 <br /> A.1yMB Ian tlmo srmml ac12A Audit Anal to Reported Value Units Method Blank Blank DF MDL ppm PQL ppm Max QL ppm <br />Metmd M.. m umlr• y <br /> I «-. N Analytes Reported <br /> rcPMS' 7 too Li Lithium mgfKg 500.00 0.26 t Ego <br />ICPMlr a 111 Be Beryllium m911Cg < < < <br />ICR.MS• 1, no B Boron mgfKg 500.00 0.5 2 Sao <br />IcP-Mr 23 1a Na Sodium mgfKg < < < <br />IcP-MV - ,n Mg Magnesium mgfKg < < < <br />rcP.MS• 27 1- A] Aluminum mgfKg < < < <br />IC"$- 20 10 Si Silicon mgfKg < < < <br />Mw . 31 10 P Phosphorus mg/Kg < < < <br />ICRMS• ]G Io K Potassium mgfKg < < < <br />Icaus• a< m Ca Calcium mgfKg e < e <br />ICP.Mr ea 10 Ti Titanium mgfKg < < < <br />ICP•M5• 51 1o y Vanandium mgfKg < < < <br />ICPMB• 52 ,o Cr 100 Chromium mgfKg < < < <br />IwMS• 55 ,o Mn Man anese mgfKg < < < <br />10P'"a' 20 Fe Iron mg/Kg < < < <br />ICP3A5• Sa 10 Co Cobalt mgfKg < c < <br />3-s' ao It Ni Nickel mgfKg < e < <br />Icp. r A3 111 Cu Copper mgfKg < < < <br />mp,Ws fib Ic Zn Zinc mg/Kg < < < <br />ICP.MS- r5 - As 100 Arsenic mglKg 500.00 0.45 1.8 11000 <br />ICRMS• 52 fro Se 20 z Selenium 0.15 .1 mgfKg < 500,00 0.15 0.6 1000 <br />ICP.M51 BB 1aa Sr Strontium mgfKg 500.110 0.026 0.1 1000 <br />lep-son Sa 10 Mo Molybdenum mg/Kg < e < <br />I.P.M. for 111 A 100 Silver mgfKg < < < <br />-.Ma• III In Cd 20 Cadmium mgfKg < < < <br />ICP-ms• 123 to Sb Antimony mgfKg < < < <br />-S• nr 1m Ba 2000 Barium mg/Kg 500.00 0.03 0.12 1000 <br />Ica-as• m2 to Hg 4 Mercury mgfKg < < < <br />1CP•Ma• 205 10 TI Thallium mg/Kg < c c <br />.P.Me• 201 10 Pb 100 Lead mgfKg < c < <br />xP.MS• 232 Ito Tit Thorium mg/Kg 600.00 0.005 0.02 500 <br />ICPMB' 23B /w U Uranium mgtKg 500.00 0.005 0.02 60o <br /> <br />•2,?..,.y, .•.. .,.?...u rraa„ 'vl'" mmgnlu°n 1.mc Can ne ep.r-. AVa11n01t At Customer s request. <br />Notes: LMB = laboratory method blank, M and MD • sample matrix replicates <br />Notes: LCS = spiked laboratory method blank, MS and MSD - spiked sample matrix replicates <br />Notes: Au Is spiked as sample prep surrogate and to facllltate analysis of Mercury, DF = Dilution Factor, <br />Notes: MDL -Method Detection Limit, PQL - Primary Quantltatlon Limit, MQL - Maximum Quantltatlon Limit, <br />Notes: < - less than MDL, J = Greater than M=L but less than PQL (4 x MDL), E = Estimated Value because it exceeds the MQL <br />Notes: n.a.=Not Applicable, Blank Space= Not Requested or Not Reported <br />Notes: RCRA TCLP Extract Limits: Ba = 100 ppm; 1Cr, As,Ag,Pb] - 5ppm; (Se, Cd] = 1 ppm; Hg = 0.2 ppm <br />Notes: "(Total RCRA limits) are 20 times the TCLP extract Iimlts because of TCLP sample size (100g) and extract volume (2000ml.). <br />"EPA SW 846 Method 1311, Revision 0, July 1992, Section 1.2: "If a total analysis of the waste demonstrates that individual analytes are not present in the waste, <br />or that they arc present but at such low coneenrntions that the appropriate regulatory levels could not possibly be exceeded, the TCLP need not be run." <br />Analyst / Reviewer <br />?0