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<br />-? Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493 <br /> <br />= <br />Wal <br />Kerr Coal Company ACZ Project ID: L59598 <br /> <br /> <br /> <br />L59598-06 WG215926 Chloride M325.2 - Colorimetric RA Relative Percent Difference (RPD) was not used for data <br /> validation because the sample concentration is too low for <br /> accurate evaluation (< 10x MDL). I <br />WG215325 Nitrate/Nitrite as N, dissolved M353.2 - Automated Cadmium RA Relative Percent Difference (RPD) was not used for data <br /> Reduction validation because the sample concentration is too low for <br /> accurate evaluation (< 10x MDL). <br />I <br />Nitrite as N, dissolved M353.2 - Automated Cadmium M1 mple <br />Matrix spike recovery was high, the method control s <br /> Reduction a <br />recovery was acceptable. <br /> M353.2 - Automated Cadmium RA Relative Percent Difference (RPD) was not used for data <br /> Reduction validation because the sample concentration is too low for <br /> accurate evaluation (< 10x MDL). <br />L59598-07 WG215926 Chloride M325.2 - Colorimetric RA Relative Percent Difference (RPD) was not used for data <br /> validation because the sample concentration is too low for <br /> accurate evaluation (< 10x MDL). <br />WG215325 Nitrate/Nitrite as N, dissolved M353.2 -Automated Cadmium RA Relative Percent Difference (RPD) was not used for data <br /> Reduction validation because the sample concentration is too low for <br /> accurate evaluation (< 10x MDL). <br />Nitrite as N, dissolved M353.2 - Automated Cadmium M1 Matrix spike recovery was high, the method control sample <br /> Reduction recovery was acceptable. <br /> M353.2 - Automated Cadmium RA Relative Percent Difference (RPD) was not used for dl to <br /> Reduction validation because the sample concentration is too low for <br /> accurate evaluation (< 10x MDL). <br />L59598-08 WG215926 Chloride M325.2 - Colorimetric RA Relative Percent Difference (RPD) was not used for data <br /> validation because the sample concentration is too low for <br /> accurate evaluation (< 10x MDL). I <br />WG215325 Nitrate/Nitrite as N, dissolved M353.2 - Automated Cadmium RA Relative Percent Difference (RPD) was not used for data <br /> Reduction validation because the sample concentration is too low for <br /> accurate evaluation (< 10x MDL). <br />Nitrite as N, dissolved M353.2 - Automated Cadmium M1 Matrix spike recovery was high, the method control sample <br /> Reduction recovery was acceptable. <br /> M353.2 - Automated Cadmium RA Relative Percent Difference (RPD) was not used for data <br /> Reduction validation because the sample concentration is too low for <br /> accurate evaluation (< 10x MDL). <br />WG215713 Residue, Filterable (TDS) @180C M160.1 - Gravimetric ZO TDS concentration is based on a final residue greater than <br /> 200 mg. <br />- - I <br />REPAD.15.06.05.01 <br />L59598: Page 12 of 17